High-plugging-performance drilling fluid composition and preparation method and application thereof
A technology of drilling fluid and composition, which is applied in the field of strong plugging drilling fluid composition and its preparation, and can solve problems such as wellbore collapse and instability, unsatisfactory effect of shale micro-nano fractures, etc.
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[0026] According to the present invention, the preparation method of described nano plugging agent comprises the following steps:
[0027] (1) dispersing the graphene nanometer in a solvent to obtain a dispersion;
[0028] (2) dispersing polyethylene glycol in the dispersion liquid for surface modification;
[0029] (3) The product obtained in (2) is washed with water, separated and dried.
[0030] According to the present invention, the particle size distribution of the nano plugging agent is 30-80nm, preferably 40-75nm, more preferably 43.5-69.7nm. In addition, the strength of the nano-blocking agent prepared by the present invention is relatively high, without biological toxicity, and it is mainly used to fill the pore space between large particles and meet the requirements of an environmentally friendly drilling fluid treatment agent; in addition, it should be noted that in the present invention In , the particle size distribution can be understood as the distribution in...
preparation example 1
[0062] This preparation example is to illustrate the preparation method of the nano plugging agent of the present invention.
[0063] Take 1g of nano-graphene material in 100mL of water and stir at a high speed under the condition of magnetic stirring rate of 900r / min. After the dispersion is uniform, take 3g of polyethylene glycol and add graphite under the condition of 60°C and magnetic stirring rate of 900r / min. The mixture was stirred continuously for 3 hours for surface modification, washed with water three times, centrifuged at 3000r / min, and baked at 60°C for 8 hours to obtain a nano-blocking agent.
[0064] Results The prepared nano-blocking agent was black powdery particles, insoluble in water, with an average particle size of 43.5nm.
preparation example 2
[0066] This preparation example is to illustrate the preparation method of the nano plugging agent of the present invention.
[0067] Take 2g of nano-graphene material in 100mL of water and stir it at a high speed under the condition of magnetic stirring rate of 800r / min. Surface modification was carried out by continuous stirring for 4 hours in the olefin solution, the mixed solution was washed with water 4 times, centrifuged at a speed of 4000r / min, and dried at 70°C for 10 hours to obtain a nano-blocking agent.
[0068] Results The prepared nano-blocking agent was black powdery particles, insoluble in water, with an average particle size of 57.6nm.
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