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A natural antibacterial method for cement composite plant fibers

A technology of cement composite material and plant fiber, applied in the field of plant fiber antibacterial, can solve the problems of high water absorption and fungal microbial corrosion, and achieve the effect of cheap raw materials and simple operation

Active Publication Date: 2020-09-04
FUJIAN AGRI & FORESTRY UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a natural antibacterial method for cement composite material plant fibers for the problems of high water absorption and fungal microbial corrosion faced by plant fiber reinforced cement materials

Method used

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  • A natural antibacterial method for cement composite plant fibers
  • A natural antibacterial method for cement composite plant fibers
  • A natural antibacterial method for cement composite plant fibers

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Preparation of cinnamon derivatives: leaves of cinnamon trees were dried in an oven at 70°C to constant weight, ground into powder by a crusher, soaked in absolute ethanol for 36 hours, filtered off the residue, and mixed with filtrate and cinnamon oil at a ratio of 1:0.2 Proportionally mixed, heated at 50°C with an intelligent magnetic stirrer, and stirred at 200 rpm until the solution remained to 75% of the original volume to obtain a cinnamon derivative.

[0030] The hemp fibers were soaked with 3.5 wt% sodium hydroxide solution for 4.5 hours, then the fibers were taken out and washed with deionized water several times until the pH of the filtered deionized water solution became neutral. Finally, at room temperature, the hemp fiber treated with sodium hydroxide solution was ventilated and dried for 36 hours, and then dried in an oven at 65° C. for 3.5 hours. The alkalized fiber was completely immersed in the cinnamon derivative for 4 hours, and after taking it out, i...

Embodiment 2

[0033] Preparation of cinnamon derivatives: cinnamon leaves were dried in an oven at 110°C to constant weight, ground into powder by a crusher, soaked in absolute ethanol for 12 hours, filtered off the residue, and mixed with filtrate and cinnamon oil at a ratio of 1:3. Proportionally mixed, heated at 85°C with an intelligent magnetic stirrer, and stirred at 120rpm until the solution remained to 85% of the original volume to obtain a cinnamon derivative.

[0034] Soak the hemp fiber with 1.5 wt% sodium hydroxide solution for 6 hours, then take out the fiber and wash it with deionized water several times until the pH of the filtered deionized water solution becomes neutral. Finally, at room temperature, the hemp fiber treated with sodium hydroxide solution was ventilated and dried for 48 hours, and then dried in an oven at 90° C. for 1 hour. The alkalized fiber was completely immersed in the cinnamon derivative for 1 hour, and after taking it out, it was ventilated and dried at...

Embodiment 3

[0037] The preparation method of cinnamon derivatives is as follows: leaves of cinnamon tree are dried in an oven at 90°C to constant weight, ground into powder by a crusher, soaked in absolute ethanol for 24 hours, filtering off the residue, and using the filtrate and cinnamon oil by 1: Mix at a ratio of 1.5, heat with an intelligent magnetic stirrer at 65°C, and stir at 180 rpm until the solution retains 80% of its original volume to obtain a cinnamon derivative.

[0038] Soak the hemp fiber with 2.5 wt% sodium hydroxide solution for 4 hours, then take out the fiber and wash it with deionized water several times until the pH of the filtered deionized water solution becomes neutral. Finally, at room temperature, the hemp fiber treated with sodium hydroxide solution was ventilated and dried for 12 hours, and then dried in an oven at 100° C. for 1 hour. The alkalized fiber was completely immersed in the cinnamon derivative for 5 hours, and after taking it out, it was ventilated...

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Abstract

The invention discloses a natural bacterium inhibiting method for a cement composite plant fiber. The plant fiber treated by using the method is greatly reduced in water absorption capacity, improvedon tensile strength and relatively strong in capacity of inhibiting the attack of fungal microorganisms. The method is mainly used for achieving the aim of mixed treating of a hemp fiber by pretreating the hemp fiber by using sodium hydroxide, dipping and alkalizing the hemp fiber by using a cinnamon derivative extracted from cinnamon leaves, and carrying out crosslinking by permeating room-temperature vulcanized silicon rubber synthesized step by step into the fiber. The water absorption capacity and tensile strength of the treated fiber are analyzed by water absorption tests and tensile property tests, and the effect of the fiber is proven by fungal microorganism corrosion experiments. The application method disclosed by the invention can be applied to corrosion resistance of a biomass material or a toughened cement composite, has no hazardous influences and cannot generate any potential hazards to environments and human beings.

Description

technical field [0001] The invention belongs to the field of plant fiber antibacterial, in particular to a natural antibacterial method for cement composite material plant fiber. Background technique [0002] Plant fibers are widely used in various composite materials and various industries (such as automotive interiors, building materials, textiles, biofuels, etc.) due to their low cost, easy availability, environmental friendliness, low density and high modulus. Since its strength and toughness can make up for the cracking problem of cement composites, more and more researches tend to plant fiber reinforced cement composites. However, the high water absorption of plant fibers, limited tensile properties and corrosion problems of fungal microorganisms have adverse effects on reinforced cementitious composites. Corrosive degradation of natural plant fibers by fungal microorganisms is a major challenge that is often neglected when reinforcing cementitious composites. As a b...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B20/02C04B20/10C04B18/24
CPCC04B20/023C04B20/1051C04B18/248Y02W30/91
Inventor 袁占辉李强周为明张明昕江一帆
Owner FUJIAN AGRI & FORESTRY UNIV