A method for preparing a large-area cobalt-nickel micro/nano periodic array structure film
A periodic array and large-area technology, applied in the field of materials, can solve the problems of complex preparation process, high price, and low degree of freedom of operation, and achieve the effect of simple preparation process, low cost, and convenient operation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0027]The first step, the preparation of the reaction solution: accurately weigh 2.3925g of cobalt nitrate hexahydrate Co(NO3)2·6H2O and 0.727g of nickel nitrate hexahydrate Ni(NO3)2·6H2Put O in a beaker, add 100 mL of deionized water, dissolve and mix, stir at room temperature for 2 hours to fully dissolve the metal soluble salt in the deionized water, then add 2mol / L of HCL solution to adjust its pH to 4 to obtain Cobalt nickel metal salt composite aqueous solution. In addition, accurately weigh 12 g of urea and place it in a beaker, add 600 mL of deionized water, stir thoroughly to dissolve, and obtain a urea solution. Under the condition of magnetic stirring, the prepared urea solution is slowly added to the cobalt-nickel metal salt composite solution to obtain a reaction solution, which is allowed to stand for use.
[0028]The second step is the preparation of the cobalt-nickel micro / nano periodic array structure film: the bird wings are treated with 1 mM HCL solution at 50°C for ...
Embodiment 2
[0033]The difference between this embodiment and the embodiment 1 lies in that: the effect of an external magnetic field of 0.05 T is not given in the preparation process of the third step.
[0034]The first step, the preparation of the reaction solution: accurately weigh 2.3925g of cobalt nitrate hexahydrate Co(NO3)2·6H2O and 0.727g of nickel nitrate hexahydrate Ni(NO3)2·6H2Put O in a beaker, add 100 mL of deionized water, dissolve and mix, stir at room temperature for 2 hours to fully dissolve the metal soluble salt in the deionized water, then add 2mol / L of HCL solution to adjust its pH to 4 to obtain Cobalt nickel metal salt composite aqueous solution. In addition, accurately weigh 12 g of urea and place it in a beaker, add 600 mL of deionized water, stir thoroughly to dissolve, and obtain a urea solution. Under the condition of magnetic stirring, the prepared urea solution is slowly added to the cobalt-nickel metal salt composite solution to obtain a reaction solution, which is al...
Embodiment 3
[0039]The difference between this embodiment and embodiment 1 is that in the second step of the preparation process, nanopaper with a pore size of 7-10 μm is used as an effective template.
[0040]The first step, the preparation of the reaction solution: accurately weigh 1.485g of cobalt nitrate hexahydrate Co(NO3)2·6H2O and 0.727g of nickel nitrate hexahydrate Ni(NO3)2·6H2Put O in a beaker, add 100mL deionized water, dissolve and mix, stir at room temperature for 3 hours to fully dissolve the metal soluble salt in deionized water, then add 0.2mol / L HCL solution to adjust its pH to 5.5. A composite aqueous solution of cobalt-nickel metal salt is obtained. In addition, accurately weigh 9 g of urea and place it in a beaker, add 300 mL of deionized water, stir thoroughly to dissolve, and obtain a urea solution. Under the condition of magnetic stirring, the prepared urea solution is slowly added to the cobalt-nickel metal salt composite solution to obtain a reaction solution, which is allo...
PUM
| Property | Measurement | Unit |
|---|---|---|
| pore size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More