Dyeing and finishing method for improving color fastness of fabric
A color fastness and fabric technology, applied in dyeing, textiles and papermaking, etc., can solve the problems of affecting the appearance of clothes, fading, easy oxidation and discoloration, etc., to improve the anti-ultraviolet radiation performance, improve the bonding strength, and improve the degree of color fixation Effect
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Embodiment 1
[0018] The specific preparation process of color-fixing finishing agent is as follows:
[0019] Step 1: Add 13.6g of p-hydroxyacetophenone into 163g of 70-80°C hot water and stir to dissolve, then keep the temperature constant and add 8.1g of formaldehyde solution with a mass concentration of 37% and stir evenly, then adjust the concentration of the solution with hydrochloric acid pH=1, dropwise add 5.04g of concentrated ammonia water dropwise, stir vigorously while adding dropwise, control the drop rate to be 6-7mL / min, keep constant temperature reaction for 5-6h after dropwise addition is complete, then carry out vacuum distillation to obtain White powder;
[0020] Step 2: Add 10g of the white powder prepared in step 1 into 150mL of ethanol and stir to dissolve, then add 16.8g of epichlorohydrin to it, heat up to 75°C, and add 3.2g of 50% hydrogen hydroxide to the reaction vessel Sodium solution, constant temperature reflux, stirring and reacting for 12 hours, then evaporat...
Embodiment 2
[0023] The specific preparation process of color-fixing finishing agent is as follows:
[0024] Step 1: Add 9.06g of p-hydroxyacetophenone into 163g of 70-80°C hot water and stir to dissolve, then keep the temperature constant and add 5.4g of formaldehyde solution with a mass concentration of 37% and stir evenly, then adjust the concentration of the solution with hydrochloric acid pH=1, add 5.04g of concentrated ammonia water dropwise to it, stir vigorously while adding, control the rate of addition to 6-7mL / min, react at constant temperature for 5-6h after the addition is complete, and then carry out vacuum distillation to obtain White powder;
[0025] Step 2: Add 10g of the white powder prepared in step 1 into 150mL of ethanol and stir to dissolve, then add 16.8g of epichlorohydrin to it, heat up to 75°C, and add 3.2g of 50% hydrogen hydroxide to the reaction vessel Sodium solution, reflux at constant temperature and stir for 12 hours, then evaporate to remove the solvent, ...
Embodiment 3
[0028] The specific preparation process of color-fixing finishing agent is as follows:
[0029]Step 1: Add 13.6g of p-hydroxyacetophenone into 163g of 70-80°C hot water and stir to dissolve, then keep the temperature constant and add 8.1g of formaldehyde solution with a mass concentration of 37% and stir evenly, then adjust the concentration of the solution with hydrochloric acid pH=1, dropwise add 5.04g of concentrated ammonia water dropwise, stir vigorously while adding dropwise, control the drop rate to be 6-7mL / min, keep constant temperature reaction for 5-6h after dropwise addition is complete, then carry out vacuum distillation to obtain White powder;
[0030] Step 2: Add 10g of the white powder prepared in step 1 into 150mL of ethanol and stir to dissolve, then add 16.8g of epichlorohydrin to it, heat up to 75°C, and add 3.2g of 50% hydrogen hydroxide to the reaction vessel Sodium solution, constant temperature reflux, stirring and reacting for 12 hours, then evaporate...
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