Anti-corrosion, anti-oxidation multi-effect cold fresh meat active nano-preservation film and preparation method thereof
A technology of nano-preservation film and cold fresh meat, applied in the field of meat preservation, can solve the problems of poor preservation effect, reduced antibacterial and antioxidant properties, difficult exposure of active substances and sudden release, etc., so as to maintain antibacterial and good antioxidant properties. and antibacterial properties, the effect of a simple preparation method
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[0040] The preparation method of the above antiseptic and anti-oxidation multi-effect cold fresh meat active nano-preservation film comprises the following steps:
[0041] 1) Take chitosan, sulfobutyl-β-cyclodextrin, ε-polylysine, compound catechin, gelatin, glycerol and transglutaminase according to the above-mentioned ratio in parts by weight;
[0042] 2) Dissolve chitosan (CS, degree of deacetylation ≥ 90%) in dilute acetic acid solution, stir magnetically at room temperature at a speed of 600r / min until completely dissolved, and filter to obtain chitosan with a mass-volume ratio of 0.01-1g / 100ml Sugar solution, for later use; adjust its pH to 5.10-5.30 before use;
[0043] 3) Dissolve sulfobutyl ether-β-cyclodextrin in water and magnetically stir until completely dissolved, filter to obtain a sulfobutyl ether-β-cyclodextrin solution with a mass-volume ratio of 0.1-1g / 100ml, and set aside;
[0044] 4) Dissolve ε-polylysine and compound catechin in sulfobutyl ether-β-cyclod...
Embodiment 1
[0122] The preparation method of anticorrosion, anti-oxidation multi-effect cold fresh meat active nano-preservation film 1 comprises the following steps:
[0123] 1) Take by weighing 6.74 parts of chitosan, 2.53 parts of sulfobutyl-β-cyclodextrin, 0.9 parts of ε-polylysine, 7.58 parts of compound catechins, 200 parts of gelatin, 40 parts of glycerol and 2 parts of transglutaminase; wherein, the compound catechin is composed of epicatechin, epigallocatechin gallate and epigallocatechin; epicatechin The weight ratio of gluten, epigallocatechin gallate and epigallocatechin is 1:0.969:0.575,
[0124] 2) Dissolve chitosan (CS, degree of deacetylation ≥ 90%) in dilute acetic acid solution, stir magnetically at room temperature at a speed of 600r / min until completely dissolved, and filter to obtain a chitosan solution with a mass-volume ratio of 0.1 / 100ml , standby; adjust its pH to 5.22 before use;
[0125] 3) Dissolve sulfobutyl ether-β-cyclodextrin in water and magnetically sti...
Embodiment 2
[0131] The preparation method of the multi-effect anti-corrosion and anti-oxidation type cold fresh meat active nano-preservation film 2 comprises the following steps:
[0132] 1) Take by weighing 6.74 parts of chitosan, 2.53 parts of sulfobutyl-β-cyclodextrin, 0.9 parts of ε-polylysine, 7.58 parts of compound catechins, 200 parts of gelatin, 40 parts of glycerol and 2 parts of transglutaminase; wherein, the compound catechin is composed of epicatechin, epigallocatechin gallate and epigallocatechin; epicatechin The weight ratio of gluten, epigallocatechin gallate and epigallocatechin is 1:0.598:0.812.
[0133] 2) Dissolve chitosan (CS, degree of deacetylation ≥ 90%) in dilute acetic acid solution, stir magnetically at room temperature at a speed of 600r / min until completely dissolved, filter to obtain chitosan with a mass-volume ratio of 0.1g / 100ml Solution, standby; adjust its pH to 5.22 before use;
[0134] 3) Dissolve sulfobutyl ether-β-cyclodextrin in water and magnetica...
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