Chemical bath method for depositing electrochromism membrane

An electrochromic and thin-film technology, applied in the direction of coating, etc., can solve the problems of unusable and uneven electrochromic thin films, and achieve the effect of low degree of hydrolysis and uniform and controllable thin film deposition

Active Publication Date: 2019-10-08
苏州伯宇光电科技有限公司
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  • Claims
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Problems solved by technology

In the process of depositing nickel oxide electrochromic film by chemical bath method, the use of the nickel oxide electrochromic film is often not uniform enough, or even unusable.

Method used

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  • Chemical bath method for depositing electrochromism membrane
  • Chemical bath method for depositing electrochromism membrane
  • Chemical bath method for depositing electrochromism membrane

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Embodiment Construction

[0027] Specific embodiments of the present invention will be further described in detail below. It should be understood that the description of the embodiments of the present invention here is not intended to limit the protection scope of the present invention.

[0028] Such as figure 1 As shown, it is a flow chart of the chemical bath method for depositing an electrochromic thin film provided by the present invention. The chemical bath method of the deposition electrochromic thin film comprises the steps:

[0029] STEP1: provide nickel sulfate and potassium persulfate, and mix the nickel sulfate and potassium persulfate to prepare the precursor solution of nickel sulfate and potassium persulfate;

[0030] The nickel sulfate is an inorganic substance, which is the source of metal nickel ions, and can dissociate nickel ions and sulfate ions during the reaction process. The potassium persulfate is also an inorganic compound and is a white crystal. The persulfate in the potas...

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Abstract

The invention discloses a chemical bath method for depositing an electrochromism membrane. The chemical bath method comprises the following steps: providing nickel sulfate and potassium persulfate, and preparing a precursor liquid of the nickel sulfate and the potassium persulfate; treating the prepared precursor liquid so as to increase the pH value of the precursor liquid; providing ammonium hydroxide, and mixing the treated precursor liquid with the ammonium hydroxide so as to obtain a mixed solution; providing FTO (fluorine-doped tin oxide) glass or ITO (indium tin oxide) glass to be plated, and soaking the FTO glass or the ITO glass to be plated into the mixed solution; taking out the plated FTO glass or the ITO glass, performing drying, and further wiping off nickel oxide deposited on the back side of the FTO glass or the ITO glass by using dilute sulfuric acid; and annealing the plated FTO glass or the ITO glass for 2-5 hours at 100-500 DEG C so as to obtain the FTO glass or theITO glass plated by the electrochromism membrane, wherein the electrochromism membrane is nickel oxide. By adopting the chemical bath method for depositing the electrochromism membrane, hydrolysis ofpersulfate can be inhibited, so that an oxygen source can be prevented from being consumed in an oxygen mode, and thus membrane deposition can be uniform and controllable.

Description

technical field [0001] The invention belongs to the technical field of electrochromism, in particular to a chemical bath method for depositing electrochromic thin films. Background technique [0002] At present, most color-adjustable sunglasses use photochromic materials. However, the transition between the transparent state and the colored state of the photochromic lens takes 5 minutes or more, and it is artificially uncontrollable, resulting in a poor user experience. Therefore, the electrochromic material with faster discoloration and artificial control provides better technical support for the discoloration lens. Moreover, the electrochromic material can also be triggered by light to change color by embedding a photoresistor, realizing two modes of manual control and automatic control. Electrochromic materials are also used in some other fields. For example, the use of electrochromic materials on smart windows can automatically block heat, thereby reducing the energy c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C17/25
CPCC03C17/25C03C2217/217C03C2217/90C03C2218/111C03C2218/328
Inventor 郭睿涵马广剑沈蒋宏李雨桐陈烨玥
Owner 苏州伯宇光电科技有限公司
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