A degradable self-repairing water-retaining and sand-fixing agent and its preparation method
A sand-fixing agent and self-repairing technology, applied in chemical instruments and methods, other chemical processes, agriculture, etc., can solve the problems of chemical sand-fixing agents being difficult to degrade, pollution in desert areas, etc., achieving good sand-fixing effect, long-term sand-fixing time, wide Application-wide effects
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Embodiment 1
[0022] Step 1, a hydrogel: 10 parts by weight of acrylamide, 3 parts of yellow gum, 10 parts of acrylic, 100 parts of water, add 0.5% of the mixture of 0.5% to potassium sulfate, add 0.3%. Unitedial age N, N'-methylene bis acrylamide, stirred for 20 min to give hydrogel to be used;
[0023] Step 2, a microcapsule is prepared: mixing the aqueous polyurethane powder and the stearate ratio of 100: 5, and the vortex gas flow refinement machine rotational speed 300 rpm is treated, and the stearic acid is sufficiently encapsulated with aqueous polyurethane powder, and then the mass concentration is 8 % Of the germinated starch, refined the mass ratio of the modified waterborne polyurethane powder and the germinated starch fluid of 3: 2; spray drying at 100 ° C, i.e., microcapsules to be used;
[0024] Step 3, preparing degradable self-repairing watergaining agent: 30 parts by weight of the hydrogel in step one, 5 parts by weight of the microcapsules in step two, 5 parts by weight of the...
Embodiment 2
[0026] Step 1, preparing a hydrogel: 15 parts of the weight of the acrylamide, 5 parts of xanthan gum, 8 parts of acrylic, 110 parts of water, add 0.5% of the mixture of 0.5% to potassium sulfate, add 0.3%. UNDER N, N'-methylene biscrylamide, stirring at least 10 min to give hydrogel to be used;
[0027] Step 2, a microcapsule is prepared: mixing the aqueous polyurethane powder and the stearate ratio of 100: 5, and the vortex gas flow refinement machine rotational speed 300 rpm is treated, and the stearic acid is sufficiently encapsulated with aqueous polyurethane powder, and then the mass concentration is 8 % Of the germinated starch, refined the mass ratio of the modified waterborne polyurethane powder and the germinated starch fluid of 3: 2; spray drying at 100 ° C, i.e., microcapsules to be used;
[0028] Step 3, preparing degradable self-repairing water saffodil: 30 parts by weight of the hydrogel in step one, 8 parts by weight of the microcapsules in step second, 5 parts by ...
Embodiment 3
[0030] Step 1, a hydrogel: 15 parts of the weight of the acrylamide, 5 parts of xanthan gum, 10 parts of acrylic, 150 parts of water, add 0.5% of the mixture of 0.5% to potassium sulfate, add 0.3%. UNDER N, N'-methylene biscrylamide, stirring at least 10 min to give hydrogel to be used;
[0031] Step 2, microcapsules: mixing the aqueous polyurethane powder and the stearate mass ratio of 100: 5, treated with vortex gas generator rotational speed 500 rpm, so that the stearic acid is sufficiently wrapped in aqueous polyurethane powder, and then the mass concentration is 8 % Of the germinated starch, refined the mass ratio of the modified waterborne polyurethane powder and the germinated starch fluid of 3: 2; spray drying at 100 ° C, i.e., microcapsules to be used;
[0032] Step three, preparing degradable self-repairing watergaining agent: 25 parts by weight of the hydrogel in step one, 9 parts by weight of the microcapsules in step second, 3 parts by weight of zeolite powder, to be ...
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