Natural Eucommia ulmoides gum (EUG) emulsion
A technology of eucommia gum and emulsion, which is applied in the field of emulsification of natural eucommia gum, which can solve the problems of destroying the regularity of molecular chains, the inability of original gum to maintain excellent performance, and destroying the crystal structure, so as to increase the scope of use, improve the machining performance, and inhibit crystallization effect
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Embodiment 1
[0028] Using the above-mentioned reaction method, 25 g of natural eucommia gum crude gum was dissolved in 250 ml of cyclohexane to prepare a eucommia gum solution with a mass concentration of 8%. Take 40ml of deionized water, dissolve 0.03g of stabilizer sodium dodecyl sulfonate, 0.12g of co-emulsifier Tween, and 5.5g of emulsifier APE-10 in order to form an aqueous solution, and add the aqueous solution to the above Eucommia gum solution , use ammonia water to adjust the solution to PH = 10, use an emulsifier to perform high-speed shear emulsification at 10000r / min, the emulsification time is 10min, and the temperature cannot exceed 45°C until the solution becomes a uniformly dispersed and stable emulsion. 0.05-0.06 atmospheric pressure, carry out vacuum distillation at 45-50° C. to remove the organic solvent, add 0.01 g of stabilizer sodium dodecylsulfonate, and mix well to prepare the natural Eucommia gum emulsion.
Embodiment 2
[0030] Using the above-mentioned reaction method, 21 g of natural eucommia gum crude gum was dissolved in 250 ml of n-hexane to form a 6% eucommia gum solution. Take 40ml of deionized water, successively dissolve 0.03g of stabilizer sodium dodecyl sulfonate, 0.12g of co-emulsifier Tween, and 5.5g of emulsifier APE-10 into water to form an aqueous solution, and add the aqueous solution to the above Eucommia gum solution , use ammonia water to adjust the solution to PH = 10, use an emulsifier to perform high-speed shear emulsification at 10000r / min, the emulsification time is 10min, and the temperature cannot exceed 45°C until the solution becomes a uniformly dispersed and stable emulsion. 0.05-0.06 atmospheric pressure, carry out vacuum distillation at 45-50° C. to remove the organic solvent, add 0.01 g of stabilizer sodium dodecylsulfonate, and mix well to prepare the natural Eucommia gum emulsion.
Embodiment 3
[0032]Adopt above-mentioned reaction method, get natural eucommia gum coarse glue 17g and dissolve in 250ml benzene and be made into the eucommia gum solution that mass concentration is 4%. Take 40ml of deionized water, successively dissolve 0.03g of stabilizer sodium dodecyl sulfonate, 0.12g of co-emulsifier Tween, and 5.5g of emulsifier APE-10 into water to form an aqueous solution, and add the aqueous solution to the above Eucommia gum solution , use ammonia water to adjust the solution to PH = 10, use an emulsifier to perform high-speed shear emulsification at 10000r / min, the emulsification time is 10min, and the temperature cannot exceed 45°C until the solution becomes a uniformly dispersed and stable emulsion. 0.05-0.06 atmospheric pressure, carry out vacuum distillation at 45-50° C. to remove the organic solvent, add 0.01 g of stabilizer sodium dodecylsulfonate, and mix well to prepare the natural Eucommia gum emulsion.
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