A kind of preparation method of coating for sand core that improves foundry quality
A technology for sand cores and coatings, which is applied in casting and molding equipment, coatings, cores, etc., can solve the problems of poor anti-sticking sand and sand washing ability of coatings, high prices, and lack of zircon powder resources.
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Embodiment 1
[0023] A method for preparing a coating for a sand core that improves casting quality, comprising the steps of:
[0024] S1. Corresponding cyclodextrin, ethylenediamine, 2-pyrenebutyric acid, N-hydroxysuccinimide, dimethylaminopyridine, and N,N-dimethylformamide according to the weight-to-volume ratio of 20g:70ml:5g: 2g: 1g: 360ml are mixed together and put into the reactor, then add dicyclohexylcarbodiimide into the reactor, stir continuously for 3 hours, take it out, put it into acetone for precipitation, and then centrifuge to take out the supernatant to get the mixture A standby;
[0025] S2, immerse the graphene nanosheets in the nitric acid solution, then filter out after ultrasonic treatment for 2 hours, then rinse with deionized water until neutral and dry for later use;
[0026] S3, putting the graphene nanosheets treated in step S2 into the reactor, then adding an acylating agent to the reactor, filtering out after ultrasonic treatment for 20min, then washing with d...
Embodiment 2
[0037] A method for preparing a coating for a sand core that improves casting quality, comprising the steps of:
[0038] S1. Cyclodextrin, ethylenediamine, 2-pyrenebutyric acid, N-hydroxysuccinimide, dimethylaminopyridine, and N,N-dimethylformamide correspond to the weight-to-volume ratio of 23g:80ml:6g: 2.6g: 1.3g: 370ml are mixed together and put into the reactor, then add dicyclohexylcarbodiimide into the reactor, stir continuously for 4 hours, take it out, put it into acetone for precipitation, and then centrifuge to take out the supernatant Get mixture A for later use;
[0039]S2, immerse the graphene nanosheets in the nitric acid solution, then filter out after ultrasonic treatment for 2.5h, then rinse with deionized water until neutral and dry for later use;
[0040] S3, putting the graphene nanosheets treated in step S2 into the reactor, then adding an acylating agent to the reactor, filtering out after ultrasonic treatment for 22min, then washing with deionized water...
Embodiment 3
[0051] A method for preparing a coating for a sand core that improves casting quality, comprising the steps of:
[0052] S1. Cyclodextrin, ethylenediamine, 2-pyrenebutyric acid, N-hydroxysuccinimide, dimethylaminopyridine, and N,N-dimethylformamide correspond to 25g:90ml:7g according to the weight-to-volume ratio: 3g: 1.5g: 380ml were mixed together and put into the reactor, then added dicyclohexylcarbodiimide into the reactor, stirred continuously for 5 hours, took it out, put it into acetone for precipitation, and then centrifuged to take out the supernatant to obtain Mixture A is standby;
[0053] S2, immerse the graphene nanosheets in the nitric acid solution, then filter out after ultrasonic treatment for 3 hours, then rinse with deionized water until neutral and dry for later use;
[0054] S3, putting the graphene nanosheets treated in step S2 into the reactor, then adding an acylating agent to the reactor, filtering out after ultrasonic treatment for 25min, then washin...
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