Stirring head for friction stir welding and fabrication method of stirring head
A friction stir welding and stirring head technology, applied in the field of powder metallurgy, can solve the problems of low production efficiency and unsuitable for industrialized production, etc.
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[0038] According to an embodiment of the present invention, a method for preparing a friction stir welding stirring head is provided, comprising the following steps:
[0039] A. Preparation of matrix alloy powder:
[0040]Prepare raw materials, according to mass percentage, the raw materials include: tungsten powder 55-85%, rhenium powder 5-15%, zirconium carbide and / or hafnium carbide powder 10-30%, tungsten powder and rhenium powder have a Fischer particle size of 2.0 ~5.0μm, the particle size of zirconium carbide and / or hafnium carbide powder is -150~-400 mesh, the purity of tungsten powder, rhenium powder and zirconium carbide and / or hafnium carbide powder are all greater than 99.5%. Mixing, the mixing machine is a three-dimensional or double-motion mixing machine, the mixing time is 3 to 10 hours, and the matrix alloy powder is obtained after the mixing is completed. Preferably, in terms of mass percentage, the raw materials include: 55-67% of tungsten powder, 5-15% of r...
Embodiment 1
[0057] Including the following steps:
[0058] A. Preparation of matrix alloy powder:
[0059] Prepare raw materials, according to mass percentage, the raw materials include: tungsten powder 70%, rhenium powder 10%, zirconium carbide powder 20%, the Fischer particle size of tungsten powder and rhenium powder are both 3.0 μm, and the particle size of zirconium carbide powder is -300 mesh The purity of tungsten powder, rhenium powder and zirconium carbide powder is greater than 99.5%. The raw materials are mixed by a three-dimensional mixer. The mixing time is 4 hours, and the matrix alloy powder is obtained after the mixing is completed.
[0060] B. Compression forming:
[0061] The matrix alloy powder obtained after step A is put into the cavity of the mold for compression forming treatment to obtain a formed billet. The forming pressure of the press forming treatment is 150MPa, and the holding time is 5s;
[0062] C. High temperature sintering:
[0063] Using a hydrogen a...
Embodiment 2
[0070] A. Preparation of matrix alloy powder:
[0071] Prepare raw materials, according to mass percentage, the raw materials include: tungsten powder 65%, rhenium powder 5%, hafnium carbide powder 30%, the Fischer particle size of tungsten powder and rhenium powder are both 2.5 μm, and the particle size of hafnium carbide powder is -200 mesh , the purity of tungsten powder, rhenium powder and hafnium carbide powder is greater than 99.5%. The raw materials are mixed with a double-motion mixer. The mixing time is 6 hours. After the mixing is completed, the matrix alloy powder is obtained.
[0072] B. Compression forming:
[0073] The matrix alloy powder obtained after step A is put into the cavity of the mold for compression forming treatment to obtain a formed billet. The forming pressure of the press forming treatment is 200MPa, and the holding time is 10s;
[0074] C. High temperature sintering:
[0075] Sinter the formed billet obtained in step B by using a hydrogen atmo...
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