Preparation method of cotton-based antibacterial composite fabric

A composite fabric, cotton-based technology, applied in the direction of repelling fibers to liquids, biochemical fiber treatment, textiles and paper making, etc. The effect of water absorption and high sterilization performance

Inactive Publication Date: 2019-12-24
JIESHOU SHUANGXIN TEXTILE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Cotton fibers are used in the preparation of close-fitting clothing because of their sweat-absorbing comfort. However, cotton fibers are prone to deformation and shrinkage after being soaked in water. At the same time, although cotton fibers have strong water-absorbing and sweat-absorbing capabilities, t

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Preparation method of cotton-based antibacterial composite fabric
  • Preparation method of cotton-based antibacterial composite fabric

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0021] Example 1:

[0022] The specific preparation process of the hydrophobic antibacterial coating agent is as follows:

[0023] ①Add 10g of diphenyl silicon diol to 170mL of acetone solution, heat up to 100-110°C and stir and mix for 20-30 minutes, then add 2.1g of p-toluenesulfonic acid and 7.2g of cis-aconitic anhydride, and heat up to 250- Reflux at 260°C for 20-22 hours to obtain a polymer solution;

[0024] ②Then the temperature in the reaction vessel was lowered to 90-95°C, and 7.6g azobisisobutyronitrile and 15.7g allyl mercaptan were added to the reaction vessel at the same time, stirred and refluxed for 1-2h and then heated to 120-130°C Reflux for 4-5h to obtain a hydrophobic antibacterial coating.

Example Embodiment

[0025] Example 2:

[0026] The specific preparation process of the antibacterial finishing agent is as follows:

[0027] Step 1: Add 11g of resorcinol to 150mL of water, while adding hydrochloric acid to it to adjust the pH=1, then add 8.1g of 37% formaldehyde solution and 16.7g of acetylhydrazine trimethyl chloride to the reaction vessel The temperature is raised to 60-70°C and the reaction is stirred for 10-12 hours, and then the solvent is evaporated and washed to neutrality to obtain phenolic hydroxyammonium chloride;

[0028] Step 2: Add 10g of the phenolic hydroxyammonium chloride prepared in step 1 to 80mL of water and stir to dissolve, then adjust the pH of the solution to 13, then add 3.5g of a 37% formaldehyde solution to it, and heat to 50-60℃ Stir the reaction for 2-3h, then add 6.2g of 37% formaldehyde solution to the reaction vessel, heat to 100-110℃ and reflux for 5-6h, then perform vacuum distillation to remove the solvent and unreacted completely Formaldehyde to ob...

Example Embodiment

[0030] Example 3:

[0031] The specific preparation process of the antibacterial finishing agent is as follows:

[0032] Step 1: Add 11g of resorcinol to 150mL of water, while adding hydrochloric acid to it to adjust the pH=1, then add 8.1g of 37% formaldehyde solution and 16.7g of acetylhydrazine trimethyl chloride to the reaction vessel The temperature is raised to 60-70°C and the reaction is stirred for 10-12 hours, and then the solvent is evaporated and washed to neutrality to obtain phenolic hydroxyammonium chloride;

[0033] Step 2: Add 10g of the phenolic hydroxyammonium chloride prepared in step 1 to 80mL of water and stir to dissolve, then adjust the pH of the solution to 13, then add 3.5g of a 37% formaldehyde solution to it, and heat to 50-60℃ Stir the reaction for 2-3h, then add 6.2g of 37% formaldehyde solution to the reaction vessel, heat to 100-110℃ and reflux for 5-6h, then perform vacuum distillation to remove the solvent and unreacted completely Formaldehyde to ob...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a preparation method of a cotton-based antibacterial composite fabric. The preparation method specifically comprises the following steps: adding treated cotton fibers into a hydrophobic antibacterial coating agent, soaking the cotton fibers with the hydrophobic antibacterial coating agent, then drying the cotton fibers, adding a silver nitrate solution with the mass concentration to soak the cotton fibers, adding the obtained fibers into an antibacterial finishing agent to soak, and steaming the fibers in hot water to obtain antibacterial hydrophobic cotton fibers; andweaving the prepared antibacterial comfortable cotton fibers into yarns, and then weaving the yarns into a fabric to obtain the cotton-based antibacterial composite fabric. An antibacterial hydrophobic layer is firstly loaded on the surfaces of the fibers, and then a porous water absorption layer is loaded on the surface of the antibacterial hydrophobic layer, so that the effect of instantaneous absorption of the cotton fibers is achieved, and the water absorption rate of the cotton fibers is improved; and moreover, the inner layer is a hydrophobic layer, after permeating out of the water absorption layer, sweat is intercepted between the water absorption layer and the hydrophobic layer by the hydrophobic layer, and does not permeate into the centers of the fibers, the water absorption layer of the outer layer contains a large number of gaps, and thus, the cotton fibers can be dried quickly.

Description

technical field [0001] The invention belongs to the field of fabric preparation and relates to a preparation method of a cotton-based antibacterial composite fabric. Background technique [0002] Cotton fibers are used in the preparation of close-fitting clothing because of their sweat-absorbing comfort. However, cotton fibers are prone to deformation and shrinkage after being soaked in water. At the same time, although cotton fibers have strong water-absorbing and sweat-absorbing capabilities, they cannot achieve fast sweat-absorbing effects. It is difficult to dry the inside, making the clothes wet and uncomfortable to wear next to the skin, especially after sweat soaking, the sweat soaks inside the fiber, making the fabric breed bacteria from the inside of the fiber center, causing the clothes to smell. Contents of the invention [0003] The purpose of the present invention is to provide a preparation method of cotton-based antibacterial composite fabric, by first loadi...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06M15/356D06M15/41D06M11/38D06M11/65D06M11/70C08F283/01C08G63/695C08G8/28C08G8/22D06M101/06
CPCC08F283/01C08G8/22C08G8/28C08G63/6958D06M11/38D06M11/65D06M11/70D06M15/3566D06M15/41D06M16/00D06M2101/06D06M2200/12C08F228/02
Inventor 杨双建龚琤琤
Owner JIESHOU SHUANGXIN TEXTILE
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