A method for preparing ball seat material for automobile guide ball pins
A technology of guiding balls and ball seats, which is applied to steering rods, vehicle parts, steering mechanisms, etc., can solve the problems of poor bonding force at the two-phase interface and difficulty in improving the notched impact strength, and achieve excellent elongation at break and notched impact The effect of excellent strength and easy promotion
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Embodiment 1
[0051] 10g of nanoscale alumina powder (average particle size = 320nm) and 5g of silane coupling agent KH570 were ultrasonically dispersed in toluene, stirred and reacted at 120°C for 4h in a nitrogen atmosphere, and then cooled to room temperature. Add 8 g of glycidyl methacrylate dissolved in toluene and a few drops of AIBN, and stir the reaction at 80° C. for 2 h in a nitrogen atmosphere. After centrifugal drying, use acetone extraction to remove unreacted coupling agent and residual toluene solvent, and finally dry to obtain modified nano-scale alumina particles. The grafting rate of glycidyl methacrylate obtained from TGA data is 13.8wt %.
[0052] Preheat 8g of modified nano-sized alumina particles at 90°C, add them to 40g of PET polyester preheated and melted at 90°C, the number-average molecular weight of PET polyester is Mn=38500 Dalton, and stir in vacuum for 2.5h, so that the two or mixed uniformly to obtain modified PET polyester.
[0053] 65g polycarbonate (numb...
Embodiment 2
[0055] 10g of nanoscale alumina powder (average particle size = 320nm) and 6g of silane coupling agent KH570 were ultrasonically dispersed in toluene, stirred and reacted at 130°C for 6h in a nitrogen atmosphere, and then cooled to room temperature. Add 12 g of glycidyl methacrylate dissolved in toluene and a few drops of AIBN, and stir the reaction at 80° C. for 2 h in a nitrogen atmosphere. After centrifugal drying, extract with acetone to remove unreacted coupling agent and residual toluene solvent, and finally dry to obtain modified nano-scale alumina particles. The grafting rate of glycidyl methacrylate obtained from TGA data is 15.4wt %.
[0056] Preheat 10g of modified nano-sized alumina particles at 90°C, add them to 40g of PET polyester that is preheated and melted at 90°C, the number average molecular weight of PET polyester is Mn=38500 Daltons, and stir in vacuum for 3h, so that the two Mix evenly to obtain modified PET polyester.
[0057] 70g polycarbonate (numbe...
Embodiment 3
[0059] Ultrasonic dispersion of 10g of nano-sized alumina powder (average particle size = 320nm) and 4g of silane coupling agent KH570 in toluene, stirred and reacted at 125°C for 3h in a nitrogen atmosphere, and then cooled to room temperature. Add 6 g of glycidyl methacrylate dissolved in toluene and a few drops of AIBN, and stir the reaction at 80° C. for 2 h in a nitrogen atmosphere. After centrifugal drying, extract with acetone to remove unreacted coupling agent and residual toluene solvent, and finally dry to obtain modified nano-scale alumina particles. The grafting ratio of glycidyl methacrylate obtained from TGA data is 11.3wt %.
[0060] Preheat 7g of modified nano-sized alumina particles at 90°C, add them to 42g of PET polyester that is preheated and melted at 90°C, the number average molecular weight of PET polyester is Mn=38500 Daltons, and stir in vacuum for 4h, so that the two Mix evenly to obtain modified PET polyester.
[0061] 60g polycarbonate (number ave...
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