High-performance ternary positive electrode material, preparation method thereof and lithium ion battery
A cathode material and high-performance technology, applied in the field of high-performance ternary cathode materials and their preparation, can solve the problems of poor cycle stability and low capacity, and achieve suitable for large-scale industrial applications, reduce the loss of Li, and improve the structure. The effect of stability
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[0043] The present invention also provides a method for preparing the above-mentioned high-performance ternary cathode material, comprising the following steps:
[0044] S1. The ternary cathode material precursor Ni x co y mn (1-x-y) (OH) 2 fully mixed with the lithium source to obtain the first mixture;
[0045] S2. Sintering the first mixture obtained in S1 to obtain LiNi x co y mn (1-x-y) o 2 Matrix material;
[0046] S3. Fully mix the matrix material obtained in S2 with MO to obtain a second mixture; wherein, the MO is MgO, Al 2 o 3 , ZrO 2 、TiO 2 , Nb 2 o 5 any of
[0047] S4. Sintering the second mixture obtained in S3 to obtain a MO-coated ternary positive electrode material;
[0048] S5. Fully mix the MO-coated ternary cathode material in S4 with distilled water, and suction filter after stirring;
[0049] S6. The material after the suction filtration in S5 is sintered three times to obtain a high-performance modified ternary cathode material.
[0050]...
Embodiment 1
[0063] This embodiment provides a high-performance ternary positive electrode material. The ternary positive electrode material is a nickel-cobalt-manganese ternary positive electrode material, and the nickel-cobalt-manganese ternary positive electrode material is LiNi coated with MO. x co y mn (1-x-y) o 2 , the expression of its chemical composition is (I): LiNi x co y mn (1-x-y) o 2 / MO(Ⅰ); where MO is Al 2 o 3 , LiNi x co y mn (1-x-y) o 2 for LiNi 0.8 co 0.1 mn 0.1 o 2 ; Al in nickel-cobalt-manganese ternary cathode material 2 o 3 The mass fraction is 0.2%.
[0064] This embodiment also provides a method for preparing the above-mentioned high-performance ternary cathode material, comprising the following steps:
[0065] S1. The ternary cathode material precursor Ni 0.8 co 0.1 mn 0.1 (OH) 2 Pour it into a high-mixer with LiOH at a molar ratio of 1:1.05, and mix thoroughly to obtain the first mixture;
[0066] S2. Put the first mixture obtained in S1 in...
Embodiment 2
[0072] This embodiment provides a high-performance ternary positive electrode material. The ternary positive electrode material is a nickel-cobalt-manganese ternary positive electrode material, and the nickel-cobalt-manganese ternary positive electrode material is LiNi coated with MO. x co y mn (1-x-y) o 2 , the expression of its chemical composition is (I): LiNi x co y mn (1-x-y) o 2 / MO(Ⅰ); Among them, MO is MgO, LiNi x co y mn (1-x-y) o 2 for LiNi 0.8 co 0.1 mn 0.1o 2 ; The mass fraction of MgO in the nickel-cobalt-manganese ternary cathode material is 0.2%.
[0073] This embodiment also provides a method for preparing the above-mentioned high-performance ternary cathode material, comprising the following steps:
[0074] S1. The ternary cathode material precursor Ni 0.8 co 0.1 mn 0.1 (OH) 2 Pour it into a high-mixer with LiOH at a molar ratio of 1:1.05, and mix thoroughly to obtain the first mixture;
[0075] S2. Put the first mixture obtained in S1 into ...
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