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Method for producing TC4 titanium alloy wide and thick plate by adopting direct rolling process

A technology of titanium alloy and wide and thick plates, which is applied in the field of non-ferrous metal materials manufacturing, can solve the problems of only 55%-65% yield, elongated layered α phase distribution, small compression ratio, etc., to solve edge crack defects, microstructure Excellent, high productivity results

Active Publication Date: 2020-04-21
ANGANG STEEL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The traditional production method of TC4 titanium alloy wide and thick plates is to first obtain titanium billets through multi-fire forging of VAR round ingots, and then pass through plate rolling mills for multi-fire rolling to obtain finished TC4 titanium alloy wide and thick plates. This process compresses The ratio is large, but the finished product rate is only 55%-65%
However, the TC4 titanium alloy plate directly rolled by the TC4 slab smelted by EB has a yield of more than 75%, but the compression ratio is small. After annealing, the conventional mechanical properties can meet the standard requirements, but its structure is elongated. The lamellar α-phase is distributed on the β-transition matrix; at the same time, there will be more serious edge crack defects when preparing wide-width plates above 2400mm

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] A method of producing TC4 titanium alloy wide and thick plate by direct rolling process, the chemical composition and content of EB ingot are: Al is 6.206wt%, V is 4.030wt%, Fe is 0.08wt%, and C is 0.0128wt% , N is 0.007wt%, H is 0.005wt%, O is 0.08wt%, and the rest is Ti and unavoidable impurities. The specific rolling process includes the following steps:

[0038] 1) Heat an EB rectangular ingot with a thickness of 220mm, a width of 1300mm, and a length of 3500mm in a continuous heating furnace. The preheating section is 700-900°C for 40 minutes, the heating section is 1100-1150°C for 120 minutes, and the soaking section is 1130-1150°C Keep warm for 120 minutes, and control the temperature at the outlet of the heating furnace at 1130-1150°C.

[0039]2) Adjust the pressure of the high-pressure water phosphorus removal tank to 16MPa for phosphorus removal. A 4300mm four-high reversing rolling mill is used for 5 passes of reciprocating rolling, the first 2 passes are h...

Embodiment 2

[0044] A method of producing TC4 titanium alloy wide and thick plate by direct rolling process, the chemical composition and content of EB ingot are: Al is 6.108wt%, V is 4.028wt%, Fe is 0.09wt%, C is 0.0128wt% , N is 0.007wt%, H is 0.005wt%, O is 0.08wt%, and the rest is Ti and unavoidable impurities. The specific rolling process includes the following steps:

[0045] 1) Heat an EB rectangular ingot with a thickness of 260mm, a width of 1300mm, and a length of 3500mm in a continuous heating furnace. The preheating section is 700-900°C for 60 minutes, the heating section is 1100-1150°C for 150 minutes, and the soaking section is 1130-1150°C Keep warm for 150 minutes, and control the temperature at the outlet of the heating furnace at 1130-1150°C.

[0046] 2) Adjust the pressure of the high-pressure water phosphorus removal tank to 16MPa for phosphorus removal. A 4300mm four-high reversing rolling mill is used for 6 round-trip rolling passes, the first 2 passes are horizontal...

Embodiment 3

[0051] A method of producing TC4 titanium alloy wide and thick plate by direct rolling process, the chemical composition and content of EB ingot are: Al is 6.102wt%, V is 4.022wt%, Fe is 0.07wt%, C is 0.0128wt% , N is 0.006wt%, H is 0.005wt%, O is 0.09wt%, and the rest is Ti and unavoidable impurities. The specific rolling process includes the following steps:

[0052] 1) Heat an EB rectangular ingot with a thickness of 300mm, a width of 1300mm, and a length of 3500mm in a continuous heating furnace. The preheating section is 700-900°C for 60 minutes, the heating section is 1100-1150°C for 180 minutes, and the soaking section is 1130-1150°C Keep warm for 150 minutes, and control the temperature at the outlet of the heating furnace at 1130-1150°C.

[0053] 2) Adjust the pressure of the high-pressure water phosphorus removal tank to 16MPa for phosphorus removal. A 5500mm four-high reversing rolling mill is used for 8 reciprocating rolling passes, the first 4 passes are horizon...

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Abstract

The invention relates to a method for producing a TC4 titanium alloy wide and thick plate by adopting a direct rolling process. The production technological process comprises the steps of EB ingot casting, primary heating, primary rolling, cooling, secondary heating, secondary rolling, annealing and aftertreatment. The steps are specifically as follows: 1) EB ingot casting: an EB furnace is used for smelting, and a TC4 titanium alloy EB slab ingot is obtained; 2) primary heating: after metal layers with the thickness of 3-5 mm on the two faces of the TC4 titanium alloy EB slab ingot are milledaway, the primary heating is conducted in a continuous heating furnace; 3) primary rolling: a blank is rolled back and forth through a wide-width medium-thickness plate rolling mill, and after hot straightening, the blank is cooled to the room temperature; 4) secondary heating; 5) secondary rolling: the blank is rolled back and forth through the wide-width medium-thickness plate rolling mill, andafter hot straightening, the blank is cooled to the room temperature; and 6) annealing. The method has the advantages of short process, low cost, high yield rate, high production efficiency, good surface quality, small differences of plate width and vertical and horizontal mechanical performance, and excellent organization.

Description

technical field [0001] The invention belongs to the field of non-ferrous metal material manufacturing, and in particular relates to a method for producing TC4 titanium alloy wide and thick plates by adopting a direct rolling process. Background technique [0002] TC4 (Ti-6Al-4V) titanium alloy contains 6wt% α-stable element Al and 4wt% β-stable element V, which is a typical α+β-type titanium alloy. It is an 800MPa high-strength titanium alloy with good plasticity, toughness and welding performance. It has broad application prospects in marine engineering, aerospace and other fields. It is currently the most widely used and most used titanium alloy in the world. Variety. In addition, in recent years, the demand for wide-width titanium plates (above 2400mm) is increasing day by day in the development of new energy development, high-end equipment manufacturing and other industries. [0003] The traditional production method of TC4 titanium alloy wide and thick plates is to fi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B21C37/02B21B3/00
CPCB21B3/003B21B2001/386B21C37/02
Inventor 张友鹏赵刚周洪庆李大航刘璇朱义轩隋松言田宇
Owner ANGANG STEEL CO LTD
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