A kind of green pepper extract and its use
A technology of green pepper and extract, applied in the field of green pepper extract and its bacteriostatic agent for Gram-positive bacteria, can solve problems such as difficult to extract fat-soluble alkaloids, achieve better antibacterial effect, improve total Alkaloid ratio, effect of improving extraction rate
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Embodiment 1
[0076] Dried green peppercorns (place of origin: Laiwu, Shandong) to moisture content ≤ 10%, and crushed to a particle size of 100 mesh to obtain green peppercorn powder. Prepare a two-phase aqueous extraction solvent, adjust pH=6.0 with 18wt% of alkyl alcohol ether glycoside AEG30, 22wt% of dipotassium hydrogen phosphate, 1.5wt% of potassium chloride and the rest of deionized water; then at 40°C Mix well, and let stand at constant temperature. According to the solid-liquid ratio of 1:12g / mL, weigh 100 mesh green pepper powder, place it in a closed microwave extraction device, add a two-phase extraction solvent, and extract at 60°C to obtain an extract. The microwave extraction conditions are: microwave power 260W; extraction time 20min. The extract was filtered with a 0.22 μm filter membrane, added to a separatory funnel and allowed to stand for phase separation to obtain an upper phase and a lower phase. Use the polysulfone ultrafiltration membrane with a molecular weight ...
Embodiment 2
[0078] Dried green peppercorns (place of origin: Laiwu, Shandong) to moisture content ≤ 10%, and crushed to a particle size of 80 mesh to obtain green peppercorn powder. Prepare a two-phase aqueous extraction solvent, adjust pH=6.5 with 20wt% of alkyl alcohol ether glycoside AEG30, 20wt% of dipotassium hydrogen phosphate, 1wt% of potassium chloride and the rest of deionized water; then at 45°C Mix well and let stand at constant temperature. According to the solid-liquid ratio of 1:10g / mL, weigh 80 mesh green Zanthoxylum bungeanum powder, place it in a closed microwave extraction device, add a two-phase extraction solvent, and extract at 65°C to obtain an extract. The microwave extraction conditions are: microwave power 240W; extraction time 18min. The extract was filtered with a 0.22 μm filter membrane, added to a separatory funnel and allowed to stand for phase separation to obtain an upper phase and a lower phase. Using a polysulfone ultrafiltration membrane with a molecul...
Embodiment 3
[0080] Dried green peppercorns (place of origin: Laiwu, Shandong) to moisture content ≤ 10%, and crushed to a particle size of 120 mesh to obtain green peppercorn powder. Prepare a two-phase aqueous extraction solvent, adjust pH=5.5 with 16wt% of alkyl alcohol ether glycoside AEG30, 24wt% of dipotassium hydrogen phosphate, 2wt% of potassium chloride and the rest of deionized water; then at 35°C Mix well and let stand at constant temperature. According to the solid-liquid ratio of 1:14g / mL, weigh 120 mesh green pepper powder, place it in a closed microwave extraction device, add a two-phase extraction solvent, and extract at 55°C to obtain an extract. The microwave extraction conditions are: microwave power 280W; extraction time 22min. The extract was filtered with a 0.22 μm filter membrane, added to a separatory funnel and allowed to stand for phase separation to obtain an upper phase and a lower phase. Purify the upper phase at an operating pressure of 0.2 MPa and room temp...
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