Blind hole-filling electroplating process, plated part obtained according to process, application of plated part, and electronic product
An electroplating process and blind hole technology, applied to electrical components, circuits, printed circuits, etc., can solve problems such as long time, difficult supply of metal ions, copper thickness of copper plating surface, etc., to avoid core and missing filling, improve Distributed across the board, avoiding the effect of filling holes
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[0153] The preparation method of the leveling agent includes: take 2g of N,N-dimethyl 1,4-butanediamine into a 50mL round neck flask, then add 5g of water to the flask and stir; place the flask in an oil bath And fix it, install a condensing reflux tube on the flask; heat the oil bath to 95℃, then slowly add 2.45g of 1,7-octadiene diepoxide compound; when the filling is completed, the temperature of the oil bath rises to 115℃ and keeps it Five hours; turn off the heating and continue to stir; cool to room temperature and collect the product, which is yellow-brown. The product is purified and dried to obtain a white powder, which is a leveling agent.
[0154] (c) Wash the test board with water: two times: the first is 3 minutes, the second is 2 minutes.
[0155] (d) Dry the test board.
[0156] (e) Cut the sample and make slices.
[0157] (f) Analyze slices and export data.
Example Embodiment
[0158] Example 1
[0159] For blind holes with a diameter of 110 μm and a depth of 85 μm, pulse filling can effectively improve the copper plating efficiency, which is 60% higher than that of DC electroplating.
[0160] The current density is 40ASF, and the total filling and plating time is 35 minutes. Use forward pulse waveform: forward current 40ASF, no direction current (reverse direction current is 0); forward current time is 40 milliseconds, reverse time is 0; pause time (current is 0 time) is 4 milliseconds; No phase difference (phase is 0), that is, the waveforms of test board A and B are synchronized; use waveform 1 for electroplating time of 25min; waveform 2 for DC waveform, continue electroplating for 10 minutes. The combined waveform is shown in Table 1.
[0161] The slice picture after electroplating is as follows Figure 5 As shown, it can be seen that: 1. The hole is filled without void; 2. The depression is less than 10 μm; 3. The copper plating thickness is 16 μm. ...
Example Embodiment
[0165] Example 2
[0166] For blind holes with relatively high depth (one-time filling of second-order blind holes), the combined positive and negative pulse combination waveform is selected. The combined waveform is shown in Table 2.
[0167] Table 2
[0168]
[0169] The slice picture after electroplating is as follows Image 6 As shown, it can be seen that: 1. The hole is filled without void; 2. The depression is less than 10 μm; 3. The copper plating thickness is 20 μm.
[0170] Image 6 Among them, the hole diameter is 102.07μm, the hole depth is 122.48μm, and the hole filling depression is 7.02μm.
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