Glossy privet fruit and radix astragali healthy energy supporting granule and preparation method thereof
The technology of Zhenqi Fuzheng and granules is applied in the field of Zhenqi Fuzheng granules and its preparation, which can solve the problem of low extraction of active components, and achieve the effects of reducing product dosage, improving economic benefits and improving product curative effect.
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[0011] The preparation method of Zhenqi Fuzheng Granules is characterized in that the steps are as follows:
[0012] (1) Raw materials: Astragalus, Ligustrum lucidum.
[0013] (2) Add 4-6 times the amount of water to the above two herbs, extract by hot reflux for 1-3 hours, filter, concentrate the filtrate, spray dry, add auxiliary materials, make granules, dry, sub-package, and make 1000 bags, Instantly.
experiment example
[0015] Determination of content Determination according to high performance liquid chromatography (general rule 0512).
[0016] Take about 15g of this product (sugar-free 2g), weigh it accurately, add 40ml of water to dissolve, put it in a separatory funnel, shake and extract 3 times with n-butanol saturated with water, 20ml each time. Combine the n-butanol extract, extract twice with the ammonia test solution, 20 ml each time, remove the ammonia test solution, evaporate the n-butanol solution to dryness, add 3 to 5 ml of water to dissolve the residue, let it cool, and absorb it through the D101 macropore Resin column (1.5 cm inner diameter, 12 cm long), elute with 50 ml of water, and discard the water. Then elute with 30ml of 40% ethanol, discard the eluate, continue to elute with 50ml of 70% ethanol, collect the eluate, evaporate to dryness, dissolve with methanol and transfer to a 2ml measuring bottle, add methanol to dilute to the mark, shake Uniform, as the test solution...
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