Preparation method of UV-moisture dual curing acid and alkali resistant conformal paint
A dual-curing, acid and alkali-resistant technology, applied in the field of coatings, can solve the problem that the shadow area cannot be cured, and achieve the effect of not affecting the ease of operation, improving stability and reducing viscosity
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Embodiment 1
[0023] Add 900kg of hydroxyl polybutadiene resin into the reaction kettle, stir and heat up to 90-100°C, vacuumize for 1 hour, pass in nitrogen to break the vacuum, cool down to 30-40°C, add 160kg of hexamethylene diisocyanate, stir Evenly, heat up to 80°C, react for 2 hours, add 1 kg of dibutyltin dilaurate, and continue to react for 3 hours to obtain an intermediate product;
[0024] The intermediate product is added to 40kg photoinitiator (configured by photoinitiator 184 and photoinitiator TPO in a mass ratio of 1:1), 120kg reactive diluent (by mass ratio of 1-nonene and 1,7-octadiene in a mass ratio of 3: 7 configuration), 1kg leveling agent BYK333 and 1kg catalyst N,N-dimethylcyclohexylamine, stir evenly to get the finished product, the reaction process and reaction principle are as follows Figure 1-2 shown.
Embodiment 2
[0026] Add 900kg of hydroxyl polybutadiene resin into the reaction kettle, stir and heat up to 90-100°C, vacuumize for 1 hour, pass in nitrogen to break the vacuum, cool down to 30-40°C, add 170kg2,4-toluene diisocyanate, stir Evenly, heat up to 80°C, react for 2 hours, add 1 kg of dibutyltin dilaurate, and continue to react for 3 hours to obtain an intermediate product;
[0027] The intermediate product is added to 40kg photoinitiator (configured by photoinitiator 184 and photoinitiator TPO in a mass ratio of 1:1), 120kg reactive diluent (by mass ratio of 1-nonene and 1,7-octadiene in a mass ratio of 3: 7 configuration), 1kg leveling agent BYK333 and 1kg catalyst N,N-dimethylcyclohexylamine, stir evenly to get the finished product, the reaction process and reaction principle are as follows Figure 1-2 shown.
Embodiment 3
[0029] Add 900kg of hydroxyl polybutadiene resin to the reaction kettle, stir and heat up to 90-100°C, vacuumize for 1 hour, blow in nitrogen to break the vacuum, cool down to 30-40°C, add 240kg of diphenylmethane diisocyanate, and stir evenly , heated up to 80°C, reacted for 2 hours, added 1 kg of dibutyltin dilaurate, and continued to react for 3 hours to obtain an intermediate product;
[0030] The intermediate product is added to 40kg photoinitiator (configured by photoinitiator 184 and photoinitiator TPO in a mass ratio of 1:1), 120kg reactive diluent (by mass ratio of 1-nonene and 1,7-octadiene in a mass ratio of 3: 7 configuration), 1kg leveling agent BYK333 and 1kg catalyst N,N-dimethylcyclohexylamine, stir evenly to get the finished product, the reaction process and reaction principle are as follows Figure 1-2 shown.
[0031] The finished product obtained as described in Implementation 1-3 is tested by the following methods:
[0032] testing method:
[0033] The f...
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