Preparation method of nano-reinforcing metal matrix composite material with high strength and toughness
A nano-reinforcement and composite material technology, which is applied in the field of preparation of high-strength nano-reinforced metal matrix composite materials, can solve the problems of reinforcement structure damage, large structural damage, and reduction of nano-reinforcement space, so as to relieve stress and strain Effects of concentrating, improving work hardening ability, and improving isotropic hardening ability
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Embodiment 1
[0032] A CNT / Al-Cu-Mg composite material was prepared, wherein the mass fraction of carbon nanotubes was 1.5%, the mass fraction of Cu was 4%, the mass fraction of Mg was 1.5%, and the mass fraction of Al was 93%.
[0033] Mix 66.25wt% pure Al powder with a median particle size of 30 μm and 25wt% 2024Al powder with 5wt% Cu powder, 1.875wt% Mg powder and 1.875wt% CNT in a mixer for 5 hours, then put it into a ball mill, and use stainless steel The ball is used as the ball milling medium, and 3wt% stearic acid is additionally added as a process control agent, the ball-to-material ratio is 20:1, ball milled at a speed of 135 rpm for 12 hours, and then ball milled at a speed of 270 rpm for 2 hours, and then CNTs are obtained Well-dispersed grade I composite powder. Mix 80 wt% of the above grade I composite powder with 20 wt% of pure Al powder without ball milling in a mixer for 5 hours to obtain grade II composite powder.
[0034] The above-mentioned grade II composite powder was f...
Embodiment 2
[0036] Prepare graphene / Al-Zn-Cu-Mg composite material, wherein, the mass fraction of graphene is 0.5%, the mass fraction of Zn is 5%, the mass fraction of Cu is 2%, the mass fraction of Mg is 2%, Al The quality score is 93%.
[0037] Mix 63.125wt% pure Al powder and 25wt% 7075Al powder with 6.25wt% Zn powder, 2.5wt% Mg powder, 2.5wt% Cu powder and 0.625wt% CNT in a mixer for 5 hours, and then Put it into a ball mill, use stainless steel balls as the ball milling medium, add 3wt% stearic acid as a process control agent in addition, the ball to material ratio is 10:1, ball mill with a speed of 150 rpm for 14 hours, and then use 300 rpm Rotate the ball mill for 2.5 hours, and then obtain a grade I composite powder with well-dispersed graphene. After uniformly mixing 75wt% of the above-mentioned grade I composite powder and 25wt% of 7075Al powder, press it into a green body with a diameter of 40 mm under a pressure of 600 MPa, and then put the green body in a vacuum sintering fu...
Embodiment 3
[0039] The nano-SiC / Al-Cu-Mg composite material was prepared, wherein the mass fraction of nano-silicon carbide was 5%, the mass fraction of Cu was 4%, the mass fraction of Mg was 1.5%, and the mass fraction of Al was 89.5%.
[0040] Mix 61.875wt% pure Al powder with a medium particle size of 30 μm and 25wt% 2024Al powder with 5wt% Cu powder, 1.875wt% Mg powder and 6.25wt% nano-SiC in a mixer for 5 hours, and then put them into a ball mill to Stainless steel balls are used as the ball milling medium, and an additional 5wt% stearic acid is added as a process control agent, the ball-to-material ratio is 15:1, ball milled at a speed of 200 rpm for 10 hours, and then ball milled at a speed of 400 rpm for 1 hour, and then obtained Grade I composite powder with well dispersed graphene. Mix 80wt% of the above grade I composite powder with 20wt% of pure Al powder without ball milling in a mixer for 5h to obtain grade II composite powder.
[0041] The above-mentioned grade II composit...
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