A kind of preparation method of polyester dye with antibacterial property
A polyester and dye technology, applied in the field of polyester dye preparation, can solve the problems of harmfulness to human body, pollution of printing and dyeing wastewater, low water solubility, etc., and achieve the effects of eliminating static electricity, improving water solubility, and improving antibacterial properties
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Embodiment 1
[0022] The specific preparation process of thiocarcinyl chloride is as follows:
[0023] Step 1: After the thiourea was dissolved in the reaction, the reaction kettle was added, stirred under an ice water bath, and then epoxy chloropropane was added thereto. 0.82, the reaction was stirred at an ice water bath for 2-3h to a normal temperature stirring reaction for 3-4 h, and then the resulting product was separated, and the obtained organic phase was dried, distilled, resulting in a cyculfide compound;
[0024] Step 2: Add a cyclooulfurium compound prepared in 10G step 1 to the reaction kettle, then adding 600 ml of concentration of 2 mol / L, a hydrochloric acid solution, stirring at room temperature for 1-2 h, then evapressive distillation to give sioane Kechlorine.
Embodiment 2
[0026] The specific preparation process of alkyl chloride is as follows: 100 g of epoxy chloropropane is added to the reactor, then a 600 ml concentration of 2 mol / L is added thereto, and the reaction is stirred at normal temperature for 1-2 h, then evaporandar, then evaporandar Kechlorine.
Embodiment 3
[0028] A method of preparing a polyester dye having antimicrobial properties, the specific preparation process is as follows:
[0029] In the first step, 100 g of dispersion pigment was added to 1 L acetone solution and dissolved, then pH = 2 of the hydrochloric acid regulating solution was added thereto, and then 23 g of the tama acid anhydride was added to the reaction vessel, and the reaction was stirred at room temperature for 7-8 h, then evaporate product After the solvent acetone in which the solvent acetone was removed, the temperature was warmed to 100-110 ° C and mixed 10-12 min and filtered, and the solid product was an unsaturated dispersion pigment, the reaction structure formula is as follows;
[0030]
[0031] In the second step, the unsaturated dispersion pigments prepared in 100 g of the first step and 900 ml of acetone were simultaneously dissolved in the reaction kettle, and 53 g of ethanol sodium ethanol and 16 g of hydroxyl phenylidecetone were added to the r...
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