Polyester resin composition for calendering, and method for producing polyester film
A technology of polyester resin and composition, which is applied in the field of polyester resin composition for calendering and polyester film preparation, can solve the problems of environmental protection, poor calendering processability, and difficult recycling, etc., and achieve low cost, excellent Effect of heat resistance and surface strength
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Embodiment 1 to 7 and comparative example 1 to 5
[0139] For the preparation of the polyester resin, a 2500 liter reactor equipped with a stirrer and outlet condenser was charged with the diol component and the dicarboxylic acid component so that the amount of final polymer was 2000 kg. Afterwards, the pressure in the reactor was raised to 2.0 kg / cm with nitrogen 2 , and the temperature of the reactor was raised to 265° C. for the reaction. In this case, the produced water is drained from the system to carry out the esterification reaction, and the reaction product is transferred to a polycondensation reactor equipped with a stirrer, a cooling condenser and a vacuum system.
[0140] 300 ppm of antimony triethylene glycol as a metal polycondensation catalyst was added to the obtained esterification reaction product, and 500 ppm of triethyl phosphate (TEP) as a stabilizer was added as an element of phosphorus. Thereafter, the temperature and pressure inside the reactor were increased to 285 to 290° C. and 50 mmHg, respectively...
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