Method for floating silicon from silicon slag
A silicon slag and silicon-poor technology, applied in the field of silicon slag treatment
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Embodiment 1
[0034] 1) Silicon slag crushing: first use a crusher to crush the silicon slag to less than 2mm, then put it into a stainless steel ball mill tank, and mill for 5 minutes;
[0035] 2) Sieving: Screen the finely ground silicon slag to obtain 10kg of 140~170 mesh silicon slag powder;
[0036] 3) Surface treatment: Then use hydrofluoric acid with a concentration of 3kg / t to carry out surface treatment on the silicon slag powder;
[0037] 4) Flotation: Add 700~750kg of hydrofluoric acid and one or two kinds of flotation wastewater filtrate to the surface-treated silicon slag, stir for 10 minutes, and add the collector cetyltrimethylammonium bromide The amount is 0.05kg / t, the foaming agent polyethylene glycol cetyl ether is added in an amount of 0.05kg / t, stirred for 7 minutes, and the bubbling switch is turned on. After the foam is abundant, then scrape and foam for 25 minutes to obtain a silicon-rich phase and Silicon-poor phase;
[0038] 5) Silicon-rich phase treatment: filte...
Embodiment 2
[0041] 1) Silicon slag crushing: first use a crusher to crush the silicon slag to less than 2mm, then put it into a stainless steel ball mill tank, and mill for 5 minutes;
[0042] 2) Sieving: Screen the finely ground silicon slag to obtain 10kg of 110~140 mesh silicon slag powder;
[0043] 3) Surface treatment: Then use hydrofluoric acid with a concentration of 3kg / t to carry out surface treatment on the silicon slag powder;
[0044] 4) Flotation: Add 700~750kg of hydrofluoric acid and one or two kinds of flotation wastewater filtrate to the surface-treated silicon slag, stir for 10 minutes, and add the collector cetyltrimethylammonium bromide The amount is 0.05kg / t, the foaming agent polyethylene glycol cetyl ether is added in an amount of 0.05kg / t, stirred for 7 minutes, and the bubbling switch is turned on. After the foam is abundant, then scrape and foam for 25 minutes to obtain a silicon-rich phase and Silicon-poor phase;
[0045] 5) Silicon-rich phase treatment: filte...
Embodiment 3
[0048] 1) Silicon slag crushing: first use a crusher to crush the silicon slag to less than 2mm, then put it into a stainless steel ball mill tank, and mill for 5 minutes;
[0049] 2) Screening: Screen the finely ground silicon slag to obtain 10kg 80~110 mesh silicon slag powder;
[0050] 3) Surface treatment: Then use hydrofluoric acid with a concentration of 3kg / t to carry out surface treatment on the silicon slag powder;
[0051] 4) Flotation: Add 700~750kg of hydrofluoric acid and one or two kinds of flotation wastewater filtrate to the surface-treated silicon slag, stir for 10 minutes, and add the collector cetyltrimethylammonium bromide The amount is 0.05kg / t, the foaming agent polyethylene glycol cetyl ether is added in an amount of 0.05kg / t, stirred for 7 minutes, and the bubbling switch is turned on. After the foam is abundant, then scrape and foam for 25 minutes to obtain a silicon-rich phase and Silicon-poor phase;
[0052] 5) Silicon-rich phase treatment: filter ...
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