4-phenoxyphenol doped carbon nitride photocatalyst and preparation method and application thereof
A phenoxyphenol, carbon nitride light technology, applied in the field of photocatalysis, can solve problems such as unfavorable industrial large-scale production, cumbersome preparation process, long preparation time, etc., and achieves improved photocatalytic performance, simple synthesis method, and improved utilization. rate effect
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Embodiment 1
[0033] A kind of preparation of 4-phenoxyphenol doped carbon nitride photocatalyst comprises the following specific steps:
[0034] Disperse 3.0g of dicyandiamide and 0.01g of 4-phenoxyphenol in 20mL of absolute ethanol respectively, after mixing, stir magnetically at room temperature for 60min, ultrasonically for 30min, then heat and evaporate to dryness under magnetic stirring at 60-80°C , the obtained solid was calcined in a muffle furnace at 540-550°C for 4h, the heating rate was 5°C / min, and the 4-phenoxyphenol-doped carbon nitride photocatalyst PCN was obtained 0.01 .
Embodiment 2
[0036] A kind of preparation of 4-phenoxyphenol doped carbon nitride photocatalyst comprises the following specific steps:
[0037] Disperse 3.0g of dicyandiamide and 0.03g of 4-phenoxyphenol in 20mL of absolute ethanol respectively, after mixing, stir magnetically at room temperature for 60min, ultrasonically for 30min, then heat and evaporate to dryness under magnetic stirring at 60-80°C , the obtained solid was calcined in a muffle furnace at 540-550°C for 4h, the heating rate was 5°C / min, and the 4-phenoxyphenol-doped carbon nitride photocatalyst PCN was obtained 0.03 .
Embodiment 3
[0039] A kind of preparation of 4-phenoxyphenol doped carbon nitride photocatalyst comprises the following specific steps:
[0040]Separately disperse 3.0g of dicyandiamide and 0.05g of 4-phenoxyphenol in 20mL of absolute ethanol. After mixing, stir magnetically at room temperature for 60min, ultrasonicate for 30min, then heat and evaporate to dryness under magnetic stirring at 60-80°C , the obtained solid was calcined in a muffle furnace at 540-550°C for 4h, the heating rate was 5°C / min, and the 4-phenoxyphenol-doped carbon nitride photocatalyst PCN was obtained 0.05 .
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