The invention discloses a visible light photocatalyst for in-situ synthesis of
hydrogen peroxide and a preparation method and application thereof, belonging to the technical field of photocatalytic material preparation; the invention adopts a wet impregnation method to impregnate a covalent
organic polymer with
chloroauric acid so that the
chloroauric acid is evenly distributed on the inner surface of the covalent
organic polymer, thereby assisting
sodium borohydride reduction to obtain gold nanoparticles and loading them on the covalent
organic polymer to synthesize a gold-loaded covalent organic
polymer (Au / COFs) visible light photocatalyst; the photocatalyst can significantly improve the
absorption capacity of visible light, has good visible light photoresponse and excellent photocatalytic performance, and can efficiently reduce
oxygen to synthesize
hydrogen peroxide in situ under visible light; the photocatalyst can be applied to the environmental field of
sustainable development and the field of clean production, sterilizes water bodies by combining with advanced oxidation technology, and the preparation method is simple, the synthesis efficiency is high, meets the actual production needs, and has high practical value and good environmental significance.