Heating element based on thermo-electronic film and preparation method thereof
A heating element, thermionic technology, applied in heating element materials, electrical components, ohmic resistance heating, etc., can solve the problems of large carbon emissions, high power of electrical equipment, low thermal efficiency, etc., to improve the thermal conversion rate, improve uniformity , reducing the effect of energy storage
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[0041] The present invention also provides a method for preparing a heating element based on a thermionic film, comprising the following steps:
[0042] Step 1, the SnCl 4 ·5H 2 O is added to the mixture of ethanol and deionized water, heated to 70-80°C, and stirred until fully dissolved; then antimony trichloride, bismuth trichloride and titanium tetrachloride are added to the solution, and stirred evenly to obtain an electric heating film liquid. Among them, the components of the electrothermal film liquid and the parts by weight of each component are: 40-45 parts of tin tetrachloride, 1.5-1.8 parts of antimony trichloride, 20-23 parts of ethanol, and 0.5-0.8 parts of bismuth trichloride 0.6-1 part of titanium tetrachloride, 28-30 parts of deionized water.
[0043] Step 2. Place the preheated tubular substrate in a high-temperature furnace, and pass the mist electrothermal film liquid into the high-temperature furnace. The mist electrothermal film liquid is deposited on t...
Embodiment 1
[0050] Step 1, the SnCl 4 ·5H 2O was added to the mixed solution of ethanol and deionized water, heated to 70°C, and stirred until fully dissolved; then antimony trichloride, bismuth trichloride and titanium tetrachloride were added to the solution, and stirred evenly to obtain an electrothermal film solution. Among them, the components of the electrothermal film liquid and the parts by weight of each component are: 40 parts of tin tetrachloride, 1.5 parts of antimony trichloride, 20 parts of ethanol, 0.5 parts of bismuth trichloride, and 0.6 parts of titanium tetrachloride , 28 parts of deionized water.
[0051] Step 2. After preheating the quartz glass tube to 400°C, place it in a high-temperature furnace, and pass the mist electric heating film liquid into the high temperature furnace. The mist electric heating film liquid is deposited on the surface of the quartz glass tube and kept for 15 minutes. After that, it is naturally cooled to obtain an electrothermal film layer...
Embodiment 2
[0054] Step 1, the SnCl 4 ·5H 2 O was added to the mixture of ethanol and deionized water, heated to 75°C, and stirred until fully dissolved; then antimony trichloride, bismuth trichloride and titanium tetrachloride were added to the solution, and stirred evenly to obtain an electrothermal film solution. Among them, the components of the electrothermal film liquid and the parts by weight of each component are: 45 parts of tin tetrachloride, 1.8 parts of antimony trichloride, 23 parts of ethanol, 0.8 parts of bismuth trichloride, and 1 part of titanium tetrachloride , 30 parts of deionized water.
[0055] Step 2. After preheating the quartz glass tube to 600°C, place it in a high-temperature furnace, and pass the mist electric heating film liquid into the high temperature furnace. The mist electric heating film liquid is deposited on the surface of the quartz glass tube and kept for 30 minutes. After that, it is naturally cooled to obtain an electrothermal film layer. Wherei...
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