Preparation process of N-carbamylglutamic acid
A carbamoylglutamic acid and a preparation process technology are applied in the preparation of organic compounds, the preparation of urea derivatives, chemical instruments and methods, etc., and can solve the problems of high cost, metabolic interference, low output efficiency, etc. Efficiency improvement and cost reduction effect
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Embodiment 1
[0026] (1) The staff uses an electronic balance to weigh according to the ratio of 8 parts of glutamic acid, 2 parts of urea, 5 parts of potassium hydroxide and 2 parts of catalyst, and then add glutamic acid, urea, potassium hydroxide and catalyst in proportion To the reaction box of the heating device, add a corresponding proportion of water treated by the ultrapure water system, and use a high-power electric stirrer to fully mix the internal raw materials, then turn on the heating device to dissolve the solid, and control the temperature at 60-65 degrees ;
[0027] (2) After reacting for 2 hours, let the solution in the reaction box of the heating device stand at room temperature for 16 to 20 hours, acidify it with concentrated hydrochloric acid, and test it with a pH meter to make pH = 6. After standing for 2 to 3 hours, pass The centrifuge carries out centrifugal filtration, and washes to neutrality, obtains crude product;
[0028] (3) recrystallize the crude product in ...
Embodiment 2
[0030] (1) The staff uses an electronic balance to weigh according to the ratio of 8 parts of glutamic acid, 2 parts of urea, 5 parts of potassium hydroxide and 2 parts of catalyst, and then add glutamic acid, urea, potassium hydroxide and catalyst in proportion To the reaction box of the heating device, add the corresponding proportion of water treated by the ultrapure water system, and use a high-power electric stirrer to fully mix the internal raw materials, and then turn on the heating device with an electric heating jacket to dissolve the solids. The temperature is 60-65 degrees;
[0031] (2) After reacting for 2 hours, let the solution in the reaction box of the heating device stand at room temperature for 16 to 20 hours, acidify it with concentrated hydrochloric acid, and test it with a pH meter to make pH = 6. After standing for 2 to 3 hours, pass The centrifuge carries out centrifugal filtration, and washes to neutrality, obtains crude product;
[0032] (3) the crude...
Embodiment 3
[0036] (1) The staff uses an electronic balance to weigh according to the ratio of 8 parts of glutamic acid, 2 parts of urea, 5 parts of potassium hydroxide and 2 parts of catalyst, and then add glutamic acid, urea, potassium hydroxide and catalyst in proportion To the reaction box of the heating device, add a corresponding proportion of water treated by the ultrapure water system, and use a high-power electric stirrer to fully mix the internal raw materials, then turn on the heating device to dissolve the solid, and control the temperature at 60-65 degrees ;
[0037] (2) After reacting for 2 hours, put the solution in the reaction box of the heating device in an ultra-low temperature refrigerator for a period of time, then acidify it with concentrated hydrochloric acid, and test it with a pH meter to make pH = 6, and then let it stand for 1 to 2 hours. , carry out centrifugal filtration by centrifuge, and wash to neutrality, obtain crude product;
[0038] (3) the crude produ...
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