Jerusalem artichoke extract-containing fruit preservative and preparation method thereof
A technology for extracts and preservatives, applied in the field of fruit preservatives and their preparation, can solve problems such as waste of resources, and achieve the effects of strong water retention, low cost, and delaying fruit decay.
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Embodiment 1
[0033] The preparation of embodiment 1 Jerusalem artichoke root extract
[0034] (1) Wash the Jerusalem artichoke root, dry it at 80°C until the moisture content of the Jerusalem artichoke root is below 8%, pulverize it with a grinder, and pass through a 40-mesh sieve to obtain the Jerusalem artichoke root particle;
[0035] (2) Heat 100 g of Jerusalem artichoke root particles with 600 g of ethanol solution with a mass fraction of 70% in a water bath to 50° C. for reflux extraction for 2 hours, and reflux extraction for 3 times, and mix the filtered filtrate to obtain an extract;
[0036] (3) The extract is vacuum rotary evaporated until it has no alcohol smell to obtain the extract;
[0037] (4) Put the extract through silica gel column chromatography, elute with ethanol-ethyl acetate solution with a volume ratio of 1:1, 2:1 and 3:1 successively, and collect ethanol-ethyl acetate solution with a volume ratio of 3:1 The fraction obtained after elution with the ester solution,...
Embodiment 2
[0038] The preparation of embodiment 2 Jerusalem artichoke tuber extract
[0039] (1) Wash the Jerusalem artichoke tubers, cut to obtain the Jerusalem artichoke slices until the thickness of each slice is less than 2mm;
[0040] (2) Heat 20 g of Jerusalem artichoke slices with 200 g of distilled water at 70° C. for 3 hours, leaching with distilled water for 3 times, mixing and concentrating the filtered filtrate to obtain an extract;
[0041] (3) Dissolve the extract with 100ml of distilled water and pour it into a separatory funnel, add 50ml of ethyl acetate into the separatory funnel, shake for 20min, let it stand for 2h, separate the upper layer of ethyl acetate extract, and the remaining lower layer of water-soluble extract Pour it back into the separatory funnel, continue to extract 10 times according to the above method, combine the 10 times of upper ethyl acetate extracts and place them in a rotary evaporator, and remove the ethyl acetate by rotary evaporation at 40 ° C...
Embodiment 3
[0042] Embodiment 3 Preparation of Fruit Preservative Containing Jerusalem Artichoke Extract
[0043] The Jerusalem artichoke root extract prepared in Example 1 is mixed with the Jerusalem artichoke tuber extract prepared in Example 2 in a mass ratio of 4:1 to form a fruit preservative.
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