Preparation method of frozen fresh walnuts
The technology of fresh walnut and walnut green fruit is applied in the field of preparation of frozen fresh walnut, which can solve the problems of sticky and mildew on the surface of the seed shell, and achieve the effects of prolonging the fresh-keeping period and slowing down the mildew.
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preparation example Construction
[0048] Examples of Preparation of Raw Materials and / or Intermediates
[0049] Chitosan: adopt oligomeric chitosan, the average molecular weight is 15000, purchased from Hebei Chuangzhiyuan Biotechnology Co., Ltd., the content is 99%;
[0050] Natamycin: Item No. 001, active matter content 99%, purchased from Zhejiang Zhonghaoxing Food Additive Co., Ltd.;
[0051] Calcium propionate: active matter content 99.8%, purchased from Hebei Chuangzhiyuan Biotechnology Co., Ltd.;
[0052] Methyl-β-cyclodextrin: average molecular weight 1331, purchased from Shanghai Yuanye Biotechnology Co., Ltd.;
[0053] Hydroxypropyl-β-cyclodextrin: average molecular weight 1380, purchased from Shanghai Yuanye Biotechnology Co., Ltd.;
[0054] 2,3-Epoxypropyltrimethylammonium chloride: purchased from Shanghai Macklin Biochemical Technology Co., Ltd.;
[0055] Isopropanol: purchased from Jinan Century Tongda Chemical Co., Ltd.;
[0056] Ethanol: Product No. ZY-036, content greater than 95%, purchas...
preparation example 1
[0058] A kind of hydrophilic natamycin, its preparation steps are as follows:
[0059] A1. Weigh 920g of methyl-β-cyclodextrin and 460g of hydroxypropyl-β-cyclodextrin into 1657ml of water to prepare a solution of β-cyclodextrin derivatives, and add 828g to the solution of β-cyclodextrin derivatives Natamycin, mix evenly to obtain a mixed solution, and place the mixed solution in a brown bottle;
[0060] A2. Ultrasonic treatment is performed on the mixed solution, the ultrasonic power is 55KW, the ultrasonic temperature is 20°C, and the ultrasonic time is 10 minutes;
[0061] A3. Shake the ultrasonically treated mixed solution until the mixed solution reaches equilibrium;
[0062] A4. Filter the mixture, put the filtrate into a brown bottle, and pre-cool at -18°C;
[0063] A5. The pre-cooled filtrate was frozen at -45°C for 20 hours.
preparation example 2
[0065] A kind of hydrophilic natamycin, its preparation steps are as follows:
[0066] A1. Weigh 1150g of methyl-β-cyclodextrin and 460g of hydroxypropyl-β-cyclodextrin into 1928ml of water to prepare a β-cyclodextrin solution, and add 966g of natamycin to the β-cyclodextrin solution , mix evenly to obtain a mixed solution, and place the mixed solution in a brown bottle;
[0067] A2. Ultrasonic treatment is performed on the mixture, the ultrasonic power is 57.5KW, the ultrasonic temperature is 19°C, and the ultrasonic time is 15 minutes;
[0068] A3. Shake the ultrasonically treated mixed solution until the mixed solution reaches equilibrium;
[0069] A4. Filter the mixture, put the filtrate into a brown bottle, and pre-cool at -18°C;
[0070] A5. The pre-cooled filtrate was frozen at -42.5°C for 22 hours.
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