5G communication-based membrane material and preparation method thereof
A membrane material and communication technology, applied in the field of membrane materials, can solve problems such as poor compatibility, easy phase separation, and affecting the service life of materials, and achieve excellent mechanical properties, improved mechanical properties and water resistance, equipment and Effects requiring low reaction conditions
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Embodiment 1
[0029] Embodiment 1 provides a film material based on 5G communication, which is characterized in that it is made of the following raw materials in parts by weight: 60 parts of adamantyl quaternary ammonium silane co-modified hyperbranched polyphenylene sulfide, hyperbranched Sulfonated polyetheretherketone 10 parts, micron-sized hollow mesoporous SiO 2 4 parts of microspheres, 2 parts of coupling agent, 0.5 parts of foaming agent, 2 parts of phosphorus pentoxide, 1 part of 2,3,5,6-tetrafluoroterephthalic acid.
[0030] The foaming agent is 3,3'-disulfonyl hydrazide diphenyl sulfone; the coupling agent is silane coupling agent KH550.
[0031] The preparation method of described adamantyl quaternary ammonium silane co-modified hyperbranched polyphenylene sulfide comprises the steps:
[0032] Step D1, adding 2-dimethylaminomethylphenol and 1-(chloromethyl)adamantane into an organic solvent, stirring and reacting at 50°C for 4 hours, and then removing the solvent by rotary evapo...
Embodiment 2
[0039] Embodiment 2 provides a film material based on 5G communication, which is characterized in that it is made of the following raw materials in parts by weight: 63 parts of adamantyl quaternary ammonium silane co-modified hyperbranched polyphenylene sulfide, hyperbranched Sulfonated polyetheretherketone 12 parts, micron-sized hollow mesoporous SiO 2 5 parts of microspheres, 2.5 parts of coupling agent, 0.7 parts of foaming agent, 2.5 parts of phosphorus pentoxide, and 1.5 parts of 2,3,5,6-tetrafluoroterephthalic acid.
[0040] The foaming agent is azoaminobenzene; the coupling agent is a silane coupling agent KH560.
[0041] The preparation method of described adamantyl quaternary ammonium silane co-modified hyperbranched polyphenylene sulfide comprises the steps:
[0042] Step D1, adding 2-dimethylaminomethylphenol and 1-(chloromethyl)adamantane into an organic solvent, stirring and reacting at 53°C for 4.5 hours, and then removing the solvent by rotary evaporation to ob...
Embodiment 3
[0049] Embodiment 3 provides a film material based on 5G communication, which is characterized in that it is made of the following raw materials in parts by weight: 65 parts of adamantyl quaternary ammonium silane co-modified hyperbranched polyphenylene sulfide, hyperbranched Sulfonated polyetheretherketone 15 parts, micron-sized hollow mesoporous SiO 2 5.5 parts of microspheres, 3 parts of coupling agent, 1 part of foaming agent, 3 parts of phosphorus pentoxide, 2 parts of 2,3,5,6-tetrafluoroterephthalic acid.
[0050] The foaming agent is barium azodicarboxylate; the coupling agent is silane coupling agent KH570.
[0051] The preparation method of described adamantyl quaternary ammonium silane co-modified hyperbranched polyphenylene sulfide comprises the steps:
[0052] Step D1, adding 2-dimethylaminomethylphenol and 1-(chloromethyl)adamantane into an organic solvent, stirring and reacting at 55°C for 5 hours, and then removing the solvent by rotary evaporation to obtain an...
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