Preparation method of porous carbonized sawdust accumulation bed material based on alkali activation and application of porous carbonized sawdust accumulation bed material in solar desalination of seawater
A stacked bed and alkali activation technology, applied in chemical instruments and methods, carbon compounds, seawater treatment, etc., can solve the problems of high cost, complex manufacturing process, high price, etc., achieve strong hydrophilicity, reduce production costs, and high efficiency The effect of solar energy absorption capacity
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Embodiment 1
[0035] A preparation method based on alkali-activated porous carbonized sawdust packed bed material, comprising the following steps:
[0036] (1) Collect wood chips produced by processing wood, and obtain wood chips with a particle size of about 100 μm after screening;
[0037] (2) Weigh about 4g of sawdust, put the sawdust into the cold-pressing mold; press the sawdust to shape with a pressure of 40MPa, and hold the pressure for 150s;
[0038] (3) Place the stacked bed of sawdust obtained in step (2) in a tube furnace, sinter in a vacuum environment at a temperature of 180°C for 25 minutes, and the temperature rise rate of the tube furnace is 8°C / min to obtain a bonded piled wood chips bed;
[0039] (4) Soak the bonded sawdust stacked bed obtained in step (3) in 0.04g / mL KOH ethanol solution for 12 minutes, filter, then wash excess KOH with ethanol and deionized water respectively, and place in a vacuum-dried box dry;
[0040] (5) Vacuum carbonize the sample obtained in st...
Embodiment 2
[0042] A preparation method based on alkali-activated porous carbonized sawdust packed bed material, comprising the following steps:
[0043] (1) Collect wood chips produced by processing wood, and obtain wood chips with a particle size of about 100 μm after screening;
[0044] (2) Weigh about 4g of sawdust, put the sawdust into the cold pressing mold; press the sawdust to shape by 40MPa pressure, and hold the pressure for 100s;
[0045] (3) Place the stacked bed of sawdust obtained in step (2) in a tube furnace, and sinter for 15 minutes in a vacuum environment at a temperature of 250°C. The temperature rise rate of the tube furnace is 5°C / min to obtain a bonded piled wood chips bed;
[0046] (4) Place the bonded sawdust stacked bed obtained in step (3) in 0.1g / ml KOH ethanol solution and soak for 6 minutes, filter, then wash the excess KOH with ethanol and deionized water respectively, and place in a vacuum-dried box dry;
[0047] (5) Vacuum carbonize the sample obtained ...
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