Rotary embedded electrostatic spinning device and spinning method

A technology of electrospinning and spinning solution, which is applied in textiles and papermaking, filament/thread forming, fiber processing, etc. It can solve the problems of few fiber diameter series, unclear diameter distribution levels, and uncontrollable distribution, etc., to achieve Less solvent volatilization, stable and continuous batch production, and the effect of improving spinning efficiency

Active Publication Date: 2021-03-16
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The technical problem to be solved by the present invention is: in the current batch electrospinning process, the number of fiber diameter series is small, the distribution is uncontrollable, and the diameter distribution level is not clear.

Method used

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  • Rotary embedded electrostatic spinning device and spinning method
  • Rotary embedded electrostatic spinning device and spinning method
  • Rotary embedded electrostatic spinning device and spinning method

Examples

Experimental program
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Effect test

Embodiment

[0030] like Figure 1-3 As shown, the rotary fitting electrospinning device provided in this embodiment includes an outer hollow cylindrical spinneret 3 and an inner hollow cylinder 4 fitted therewith, and the spinning liquid supply device includes a digitally controlled micro-injection pump 1 connected to a syringe 2. The hose is connected to the inner hollow cylinder 4, and there are four different types of openings on the outer hollow cylinder spinneret 3, which are driven to rotate by the servo motor 6, and the inner hollow cylinder 4 is connected to the high-voltage positive electrode, when the outer hollow cylinder spinneret When the opening of 3 is connected with the opening of inner hollow cylinder 4, and the voltage exceeds a critical value, multiple electrospinning jets will be generated at the connected opening.

[0031] The inner hollow cylinder 4 is fixed horizontally and does not rotate with the rotation of the outer hollow cylinder spinneret, and the high-voltag...

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Abstract

The invention discloses a rotary embedded electrostatic spinning device and a spinning method. The rotary embedded electrostatic spinning device comprises an outer hollow cylinder spinning nozzle, aninner hollow cylinder, an injector used for injecting spinning liquid into the inner hollow cylinder, a numerical control micro-injection pump used for controlling the injector, a high-voltage positive electrode connected with the inner hollow cylinder and the like. The spinning method comprises the steps that the spinning solution is injected into the inner hollow cylinder, when the spinning solution rises and the liquid level is higher than an opening in the top of the inner hollow cylinder, a servo motor is started to drive the outer hollow cylinder spinning nozzle to rotate the high-voltage positive electrode is opened and connected, voltage is increased, a plurality of electrostatic spinning jet flows is generated above the opening, and an electrostatic spinning process is started; and the electrostatic spinning jet flows are received through a collecting device. The spinning solution can form liquid films in different states on the openings in different forms, and then the jet flows with different fineness are generated, so that a nanofiber film with four or more diameter distributions and distinct levels can be prepared in one step under the condition without using various spinning solutions and without adjusting spinning parameters.

Description

technical field [0001] The invention belongs to the technical field of electrostatic spinning and textile machinery, and in particular relates to a rotating and embedded electrostatic spinning device and method. Background technique [0002] Electrospinning is one of the most effective ways to prepare nanofiber materials. Compared with the preparation techniques of nanomaterials such as stretching method, template synthesis method, and self-assembly, electrospinning has the advantages of simple operation, short preparation process, and wide selection of materials. advantage. [0003] Compared with traditional textile fiber materials, nanofiber materials have many properties that are difficult to develop on a large scale due to their extremely small scale. [0004] The existing characteristics, such as obvious surface and interface effects, unique small size effect, large specific surface area and extremely high porosity, etc. Therefore, nanofiber materials have a wider ran...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D5/00
CPCD01D5/0069D01D5/0092
Inventor 王富军李皖李超婧刘来俊王程毅王璐
Owner DONGHUA UNIV
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