A method for removing chlorine from desulfurization wastewater drying ash in coal-fired power plants
A technology for desulfurization wastewater and coal-fired power plants, applied in chemical instruments and methods, solid waste removal, transportation and packaging, etc., can solve the problems of large output of dried ash, waste of resources, low chlorine removal rate, etc. Good chlorine effect, cost saving, and easy removal
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Embodiment 1
[0027] Weigh 3g of ash slag that has been sieved by a dry ball mill, accurately weigh it to 0.1g, put it in a 100ml beaker, and pickle it with 0.8mol / L acetic acid solution according to the solid-to-liquid ratio of 1:10. Stir in a magnetic stirrer at room temperature for 5 minutes, then pour the mixture into a centrifuge tube, and centrifuge at 1000 r / min for 15 minutes. Pour off the lotion, continue to add acid solution into the centrifuge tube, place it in an ultrasonic cleaner for 10 minutes of ultrasonic oscillation, then pour it into a beaker for magnetic stirring for 10 minutes, and then repeat the above steps for centrifugal ultrasonication.
[0028] Remove the lotion, add deionized water to the centrifuge tube and perform ultrasonic oscillation for 10 minutes, then use a Buchner funnel and qualitative filter paper to perform suction filtration, and then wash and filter twice to obtain the filter residue. The filter residue was dried in an oven at 105° C. to a constant ...
Embodiment 2
[0031] Weigh 3g of the ash slag that has been sieved by a dry ball mill, accurately weigh it to 0.1g, put it in a 100ml beaker, and pickle it with 0.6mol / L acetic acid solution according to the solid-to-liquid ratio of 1:15. Stir in a magnetic stirrer at room temperature for 5 min, then pour the mixture into a centrifuge tube, and centrifuge at 500 r / min for 20 min. Pour off the lotion, continue to add acid solution into the centrifuge tube, place it in an ultrasonic cleaner for 10 minutes of ultrasonic oscillation, then pour it into a beaker for magnetic stirring for 10 minutes, and then repeat the above steps for centrifugal ultrasonication.
[0032] Remove the lotion, add deionized water to the centrifuge tube and perform ultrasonic oscillation for 10 minutes, then use a Buchner funnel and qualitative filter paper to perform suction filtration, and then wash and filter once more to obtain the filter residue. The filter residue was dried in an oven at 105° C. to a constant w...
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