Manufacturing method of display screen cover plate

A manufacturing method and a technology of a display screen, which are applied in manufacturing tools, glass tempering, glass manufacturing equipment, etc., can solve problems such as long time consumption, reduction of chemical strengthening strength, difficulty in wide-range adjustment of particle spacing, etc., to reduce ion exchange time , Reduced ion blockage, good ion exchange effect

Active Publication Date: 2021-04-02
(CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The former will generate more polishing waste liquid, which is not conducive to environmental protection; the latter not only has limited ability to adjust the warpage, but also reduces the strength of chemical strengthening. The reason is that the chemical strengthening of the existing technology is usually below the transition temperature of glass. The subsequent annealing is a process of slowly cooling the glass from the ion exchange temperature to room temperature in order to relieve the stress. During the entire annealing process, even at the higher temperature stage at the beginning of the annealing, the particles in the glass network structure are mostly in the Compared with the inert state, it is difficult to adjust the particle spacing in a large range. Therefore, the latter can only reduce the compressive stress gap between the two sides of the glass. If the warpage is large, it is difficult to reduce the warpage to the ideal range; on the other hand, although During the annealing process, most of the particles in the glass network structure are in an inert state, but the cations located outside the network structure can diffuse relatively freely, especially after chemical strengthening, the potassium ions on the surface of the glass are in a state higher than that in the interior. , there is always a tendency to diffuse to the inside, and the diffusion coefficient of ions is related to temperature. The higher the temperature, the greater the diffusion coefficient. time, diffuse into the glass with a higher diffusion coefficient, and finally reduce the concentration of potassium ions on the glass surface, thereby reducing the strength of the glass due to chemical strengthening

Method used

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Examples

Experimental program
Comparison scheme
Effect test

specific Embodiment 1

[0020]In the present embodiment, an ultra-thin glass manufactured in float is employed, and the glass thickness is 1.1 mm, and the glass viscosity value is 10.10~ 108Pa • Second correspondence is 610 ~ 660 ° C, 1013.6~ 1012.4Pa • Second temperature range 473 ~ 520 ° C, viscosity value 1013.6Pa • Second correspondence temperature The temperature ranges from 40 to 70 ° C in a temperature range of 403 to 433 ° C, and a sample of 2 sheets 24 of 248 x 178 mm was obtained after cutting of grinding, wherein the sample A is used in the present invention for comparative test.

[0021]this invention:

[0022]A method of making a display cover, including the following steps:

[0023](1) Heating, the sample A is placed vertically in the fixture to 610 to 660 ° C, preferably 630 ° C in the present embodiment;

[0024](2) Asymmetric quench, use different temperatures silicone oil to quench the tin and air surfaces of the glass, in which the temperature of the silicone oil acting on the tin surface is 200 ° C...

specific Embodiment 2

[0037]In the present embodiment, the same two samples as those of the specific examples are selected, wherein the sample C is used in the present invention, and the sample D is used for comparative tests.

[0038]this invention:

[0039]A method of making a display cover, including the following steps:

[0040](1) Heating, placing the sample C vertically in the fixture to 610 to 660 ° C, preferably 650 ° C in the present embodiment;

[0041](2) Asymmetric quench, the particle size is 150 μm alumina fine particles as the cooling medium, wherein the temperature of the alumina fine particles acting on the tin surface is 250 ° C, which is 250 ° C, which is 250 ° C, which is 250 ° C, which is 250 ° C. The aluminum fine particle temperature is 200 ° C, the alumina fine particle temperature of the air surface is 450 ° C, and the alumina fine particles of different temperatures are sprayed into the tin and air surfaces of different temperatures, and when the glass temperature is quenched to 473 ~ 520. ...

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Abstract

The invention provides a manufacturing method of a display screen cover plate. The manufacturing method comprises the steps of (1) heating glass to a temperature corresponding to a viscosity value of10<10>-10<8>Pa.s; (2) synchronously quenching the tin surface and the air surface of the glass by using cooling media with different temperatures, and stopping quenching when the temperature of the glass is quenched to a temperature range corresponding to the viscosity value of 10<13.6>-10<12.4>Pa.s; (3) heating the dried pure nitrogen until the temperature is 40-70 DEG C lower than the temperature corresponding to the viscosity value of 10<13.6>Pa.s, and purging and cleaning the two sides of the glass with nitrogen until the temperature of the glass is equal to the temperature of the nitrogen; (4) heating potassium nitrate of which the purity is greater than 99.9% to the temperature of the nitrogen to form potassium nitrate molten salt, then immersing the glass into the potassium nitratemolten salt for ion exchange, and annealing to room temperature after the ion exchange is finished; and (5) conducting cleaning, drying and the like to obtain the display screen cover plate. The method has the advantages that the glass does not need to be ground, and the chemical strengthening strength of the glass cannot be reduced.

Description

Technical field[0001]The present invention relates to the field of display cover cover, and is specifically a method of fabricating a display cover.Background technique[0002]The display cover is usually made of ultra-thin glass (0.10 mm-1.8 mm), cutting, edging, grinding, chemical strengthening, etc., of which chemical strengthening is immersed in glass potassium nitrate, potassium ions in the molten salt The sodium ions in the glass were generated from ion exchange, and the provering effect of potassium ions produced a pressure stress in the glass surface, thereby increasing the strength of the glass.[0003]When the cover is made of ultra-thin glass by float, since the float glass is in contact with the tin liquid, the surface thereof will have a certain degree of otters, which is called "tin surface", and the other side The contact air is called "air surface", in ion exchange, since the "tin surface" sodium ion content is relatively low, the ion exchange is affected, so that the io...

Claims

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Application Information

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IPC IPC(8): C03B27/004C03B27/02C03C21/00
CPCC03B27/004C03B27/024C03C21/002Y02P40/57
Inventor 王东鲍田汤永康甘治平李刚杨扬姚婷婷王金磊苏文静
Owner (CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD
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