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Preparation method of palm oil fatty acid magnesium

A technology of fatty acid magnesium and palm oil, which is applied in the field of preparation of palm oil fatty acid magnesium, can solve the problems of reducing the pulverizing effect, reducing the sharpness of the pulverizing knife, side effects and the like

Active Publication Date: 2021-05-11
厦门旭翀生物医药科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Magnesium stearate is commonly used as a film coating for tablets. In addition to its lubricating effect, it can also help release the active ingredients in the drug at a precise time as needed, but excessive intake of magnesium stearate can also cause some side effects
Magnesium palm oil fatty acid has a better effect, but the saponification rate and purity of the final product are not satisfactory in common methods, which will lead to a large amount of waste of palm oil
In the production process of existing magnesium stearate, magnesium stearate needs to be pulverized before it is used as medicine in order to improve magnesium stearate, but the magnesium stearate material will produce friction with the blade during the pulverization process, which will cause magnesium stearate The powder sticks to the surface of the crushing knife at high temperature. If it is not cleaned in time, when the magnesium stearate powder cools down, the magnesium stearate powder that sticks to the crushing knife and has not been cleaned in time will absorb the moisture in the surrounding air and condense on the Smash on the blade face and blade, reduce the sharpness of the shredding knife and reduce the shredding effect

Method used

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  • Preparation method of palm oil fatty acid magnesium
  • Preparation method of palm oil fatty acid magnesium
  • Preparation method of palm oil fatty acid magnesium

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Embodiment 1 has introduced a kind of preparation method of palm oil fatty acid magnesium, as Figure 1-3 Shown, a kind of preparation method of palm oil fatty acid magnesium comprises seat plate 1, pulverizer housing 2, motor 3 and discharge pipe 4; Described preparation equipment also comprises blade cleaning assembly 5 and installation assembly 6; Described seat The upper surface of the plate 1 is fixedly connected with a pulverizer housing 2, and one side of the pulverizer housing 2 is fixedly connected with a horizontally arranged motor 3; the lower end of the pulverizer housing 2 is fixedly connected with a discharge pipe 4 , the discharge pipe 4 runs through the seat plate 1;

[0044] Such as Figure 4-7 As shown; the upper end of the pulverizer housing 2 is fixedly connected with a blade cleaning assembly 5; the blade cleaning assembly 5 includes a handle 501, a pair of guide sleeves 502, a pair of springs 503, a pair of movable rods 504 and blade cleaning Bru...

Embodiment 2

[0054] Embodiment 2 is an improvement on the basis of Embodiment 1, as Figure 8-10 As shown, wherein, the mounting plate 507 is provided with a through hole 7 vertically penetrating the mounting plate 507 with the same shape as the limiting plate 604, and the upper surface of the mounting plate 507 is also provided with a limiting groove 8, so Part of the limiting groove 8 intersects with the through hole 7; each of the mounting plates 507 is provided with a pair of mounting components 6, and the mounting components 6 include a fixed sleeve 601, a torsion bar 602, a button handle 603 and a limiting plate 604 , the bottom end of the fixed sleeve 601 is fixedly connected to the upper surface of the blade cleaning brush 505 through the second mounting plate 605, and the fixed sleeve 601 is perpendicular to the blade cleaning brush 505; Baffle 1 606; the bottom end of the torsion bar 602 is fixedly connected with an annular baffle 2 607, the top of the torsion bar 602 passes thro...

Embodiment 3

[0063] Embodiment 3 is an improvement on the basis of Embodiment 1, as Figure 11 As shown, the torsion bar 602 is also sleeved with a spring 9, the spring 9 is located inside the fixed sleeve 601, one end of the spring 9 is against the upper surface of the annular baffle 607, and the spring 9 The other end of the other end is against the lower surface of the ring baffle 1 606; the spring 9 is a compression spring; After the button handle 603 and the limiting plate 604 pass through the through hole, the knob handle 603 is rotated until the limiting plate 604 is located directly above the limiting groove 8, and then the button handle 603 is released, and the limiting plate 604 is positioned on the spring Two 9 are tightly engaged in the limiting groove 8 under the stretching action.

[0064] In this embodiment, further, by adding a spring 2 9 between the fixed sleeve 601 and the torsion bar 602, after the button handle 603 is released, the limit plate 604 is always tightly eng...

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PUM

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Abstract

The invention provides a preparation method of palm oil fatty acid magnesium. The preparation method of the palm oil fatty acid magnesium comprises the following steps of 1, dropwise adding hydrogen peroxide into palm oil, magnesium oxide, magnesium hydroxide, magnesium laurel sulfate and a 90-percent ethanol solution, and dispersing for 2 hours through strong pulping; 2, adding natural activated carbon and sodium hydroxide, heating to a reflux state, and keeping for 2 to 4 hours; 3, controlling the temperature to be 40 to 50 DEG C, and performing reduced pressure distillation to remove ethanol and water; 4, keeping the vacuum degree of minus 0.005 Mpa to minus 0.01 Mpa, increasing the temperature to 100 to 120 DEG C, and keeping the temperature for 1 to 1.5 h; and 5, adding deionized water, stirring, then filtering while the solution is hot, and evaporating the filtrate until the solution is dry.

Description

technical field [0001] The invention belongs to the technical field of biomedicine preparation, in particular to a preparation method of palm oil fatty acid magnesium. Background technique [0002] Magnesium stearate is an additive widely used in health products. It is generally made from hydrogenated vegetable fats, which can hinder the absorption of nutrients and immunity, and may also have other toxic effects. Magnesium stearate is commonly used as a film coating for tablets. In addition to its lubricating effect, it can also help release the active ingredients in the drug at a precise time as needed, but excessive intake of magnesium stearate can also cause some side effects. Magnesium palm oil fatty acid has a better effect, but the saponification rate and the purity of the final product in common methods are not satisfactory, which will lead to a large amount of waste of palm oil. In the production process of existing magnesium stearate, magnesium stearate needs to be...

Claims

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Application Information

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IPC IPC(8): B02C18/06B02C18/16B08B1/02B08B13/00A61K47/12
CPCB02C18/06B02C18/16B08B13/00A61K47/12B08B1/12B08B1/20Y02W30/74
Inventor 曹生们
Owner 厦门旭翀生物医药科技有限公司