Caprolactam production wastewater treatment system and method

A technology for treatment system and production wastewater, applied in water/sewage treatment, natural water treatment, oxidized water/sewage treatment, etc. It can solve the problems of low COD elimination rate, increase follow-up work, and high equipment requirements, and increase the phase interface area. , the effect of saving costs and reducing energy consumption

CN113087252AActive Publication Date: 2021-07-09NANJING YANCHANG REACTION TECH RES INST CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Publication Date
2021-07-09

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Abstract

The invention provides a caprolactam production wastewater treatment system and method. The treatment system comprises a raw water tank, a wastewater heat exchanger, a wastewater heater and an oxidation reactor which are sequentially connected, wherein a material inlet, a material outlet, a heat source inlet and a heat source outlet are formed in the wastewater heat exchanger; oxidized water from the oxidation reactor enters the wastewater heat exchanger from the heat source inlet, the heat source outlet is connected with a finished product tank, the material inlet is connected with the raw water tank, the material outlet is connected with the wastewater heater, a micro-interface generation system is arranged in the oxidation reactor, and the micro-interface generation system is used for dispersing the crushed gas into bubbles. According to the treatment system, after the micro-interface generator is arranged, the contact of thereaction phase interface is improved, and a good wastewater treatment effect can be obtained without using a catalyst or by adding a small amount of the catalyst.
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Description

technical field

[0001] The invention relates to the field of caprolactam production wastewater treatment, in particular to a treatment system and method for caprolactam production wastewater. Background technique

[0002] Caprolactam is an important chemical material. Its main purpose is to produce polyurethane through polymerization, which can be further processed into fibers, plastics, films, etc. The main domestic production methods of caprolactam are the toluene method and the benzene method, but in the end, caprolactam is obtained through the liquid-phase Beckmann rearrangement reaction of cyclohexanone oxime. This process has a fast reaction speed and high conversion rate, but the wastewater produced by it is difficult to treat. larger. Wastewater mainly contains caprolactam, ammonium sulfate, acetic acid, toluene, benzoic acid, cyclohexane carboxylic acid, cyclohexane carboxylic acid sulfonic acid, hexahydrobenzoic acid, cyclohexane and other components. There are ma...

Examples

Embodiment

[0058] refer to figure 1 Shown is a caprolactam production wastewater treatment system according to an embodiment of the present invention, which includes a raw water tank 10 , a wastewater heat exchanger 50 , a wastewater heater 60 , an oxidation reactor 70 and an air compressor 74 connected in sequence.

[0059] Wherein, the waste water heat exchanger 50 has a material inlet 51, a material outlet 52, a heat source inlet 53, and a heat source outlet 54 respectively, and the oxidized water coming out of the oxidation reactor 70 enters the waste water heat exchanger 50 from the heat source inlet 53. The heat source outlet 54 is connected to the finished product tank 90, the material inlet 51 is connected to the raw water tank 10, and the material outlet 52 is connected to the waste water heater 60. In the waste water heat exchanger 50, the oxidized water after the oxidation reactor 70 is reacted and the The treated caprolactam production wastewater is heat-exchanged, so as to a...