Proton exchange membrane fuel cell catalyst synthesis method
A proton exchange membrane and fuel cell technology, applied in battery electrodes, circuits, electrical components, etc., can solve problems such as high cost, substandard service life of metal bipolar plates, and hydrogen energy transportation and storage problems, reducing production costs. , The effect of low monolithic battery loading and improving catalyst performance
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[0045] 125 mg of dried Pt / C precursor and 30 mg of hexahydrate cobalt were dispersed in 20 ml of water, and it was more than 1 hour.
[0046] Configure 20 mg / ml of NABH 4 Aqueous solution, take 4 mlnabh 4 The aqueous solution was added dropwise to the dispersion. After adding NABH 4 The mixture was stirred for 12 h, and then the mixture was filtered with a sand core, and 300 ml of water was used, three times, and then the CO-containing Pt / C sample was dried.
[0047] The dried CO-containing PT / C sample was placed in a tubular furnace, under argon conditions, the water temperature rate was 5 ° C / min, and then naturally cooled to room temperature after heating to 400 ° C for 2 hours to obtain a PTCO containing cobalt particles. / C alloy catalyst.
[0048]The 10 ml solution was equipped with 2 mL and 3 ml of concentrated nitric acid, respectively, and the PTCO / C alloy catalyst containing cobalt particles was treated with a cobalt particles. After stirring for 12 h, the d...
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