Intelligent adsorption/release system based on excitation response polymer and preparation method of intelligent adsorption/release system
An excitation-response and systematic technology, which is applied in the fields of alkali metal compounds, chemical instruments and methods, alkali metal oxides/hydroxides, etc., can solve the problems of inability to achieve controllable positioning and timing adsorption, and achieve easy modification and modification. Composite, easy to expand, and good designability
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Embodiment 1
[0023] Example 1: Weigh 6g of polyvinyl alcohol with a degree of alcoholysis of 87-89 mol%, add it to 100ml of deionized water at room temperature and stir to make it fully swell, then slowly heat to 100 o After C, keep constant temperature, stir and disperse, fully dissolve until the solution is uniform and clear as a whole, then adjust the pH value to 3.5 after natural cooling to room temperature, and fully stir to obtain a polyvinyl alcohol solution. Add 0.5wt% carbon nanofibers to the prepared polyvinyl alcohol solution, stir mechanically to make them uniformly dispersed, then add 2.5vol% glutaraldehyde and mechanically stir for 20 min to obtain carbon nanofiber / polyvinyl alcohol excitation-response composites The pre-polymerization solution is poured into the mold and left to stand for a period of time, followed by vacuum freeze-drying treatment to obtain the carbon nanofiber / polyvinyl alcohol excitation-response composite material, figure 1 Shown are its macroscopic morp...
Embodiment 2
[0024] Example 2: Weigh 6g of polyvinyl alcohol with a degree of alcoholysis of 87-89 mol%, add it to 100ml of deionized water at room temperature and stir to make it fully swell, then slowly heat to 100 oAfter C, keep constant temperature, stir and disperse, fully dissolve until the solution is uniform and clear as a whole, then adjust the pH value to 3.5 after natural cooling to room temperature, and fully stir to obtain a polyvinyl alcohol solution. Add 5wt% carbon nanotubes to the prepared polyvinyl alcohol solution, stir mechanically to make them uniformly dispersed, then add 5vol% glutaraldehyde and mechanically stir for 20 min to obtain the prepolymerized carbon nanotube / polyvinyl alcohol excitation-response composite material After being poured into the mold and left to stand for a period of time, vacuum freeze-drying was carried out to obtain the carbon nanotube / polyvinyl alcohol excitation-response composite material. At room temperature, add 5wt% PC to the mixed sol...
Embodiment 3
[0025] Example 3: Weigh 6g of polyvinyl alcohol with a degree of alcoholysis of 87-89 mol%, add it to 100ml of deionized water at room temperature and stir to make it fully swell, then slowly heat to 100 o After C, keep constant temperature, stir and disperse, fully dissolve until the solution is uniform and clear as a whole, then adjust the pH value to 3.5 after natural cooling to room temperature, and fully stir to obtain a polyvinyl alcohol solution. Add 0.5wt% carbon nanofibers to the prepared polyvinyl alcohol solution, stir mechanically to make them uniformly dispersed, and then add 5vol% glutaraldehyde and mechanically stir for 20 min to obtain the carbon nanofiber / polyvinyl alcohol excitation-response composite material The poly solution is poured into a mold and left to stand for a period of time, followed by vacuum freeze-drying to obtain a carbon nanofiber / polyvinyl alcohol excitation-response composite material. At room temperature, add 5wt% PC to the mixed solutio...
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