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86 results about "Composite microstructure" patented technology

Preparation method and application of super-hydrophobic and adhesion-adjustable surface with micro-nano composite structure

The invention relates to a preparation method for a super-hydrophobic and adhesion-adjustable surface with a micro-nano composite structure. The preparation method comprises the following steps: a, preparing a dual-level composite microstructure template according to wetting characteristics needed by a product surface; b, preparing a solution from a hydrophilic / hydrophobic nanoparticle and absolute ethyl alcohol according to adhesion characteristics needed by the product surface, immersing the dual-level composite microstructure template into the solution, carrying out ultrasonic dispersion, then taking the treated microstructure template out and drying the treated microstructure template so as to obtain a three-level micro-nano composite structure template; c, fixing the obtained template on the surface of a die cavity, injecting high-molecular melt into the cavity by using an injection machine, carrying out pressure maintaining and then carrying out cooling and molding; and d, separating a molded high-molecular product from an injection die by using a demolding apparatus. The hydrophilic / hydrophobic nanoparticle is adhered on the surface or embedded into the surface layer of the dual-level composite microstructure on the surface of the molded high-molecular product, and the molded high-molecular product surface has the characteristics of super-hydrophobicity and adjustable adhesion and can realize flexible switching between a lotus leaf effect and a petal effect.
Owner:SOUTH CHINA UNIV OF TECH

Nano-porous aerogel/fiber composite super thermal insulation material and preparation method thereof

The invention discloses a nano-porous aerogel / fiber composite super thermal insulation material and a preparation method thereof. The aerogel / fiber composite super thermal insulation material comprises silicon dioxide aerogel, alumina micro powder, zirconium oxide fibers and opacifying agent of titanium dioxide. The preparation method comprises that organic solvent, cross-linking agents and organic monomers make up pre-mixed solution according to a certain proportion, the silicon dioxide aerogel, the alumina micro powder, the zirconium oxide fibers, pore-forming agents, suspending agents and the titanium dioxide make up slurry through a ball milling process according to a certain proportion, then a certain amount of initiating agents and a certain amount of catalytic agents are dropwise added into the slurry through vacuum bubble removal, composite material in-situ solidification is achieved through a gel injection moulding process, and then demoulding, vacuum drying and degreasing glue discharging are conducted. The nano-porous aerogel / fiber composite super thermal insulation material has a nano-porous / reinforced fiber composite microstructure, the heat conductivity is 0.040-0.046W*m<-1>*K<-1> (298K), and the flexure strength is as high as 12-14MPa. Preparation processes are simple, industrialized application is easily achieved on a large scale, and the nano-porous aerogel / fiber composite super thermal insulation material is suitable for thermal protection of aerospace, military affairs and severe rugged environments.
Owner:JIANGSU ZHONGLEI ENERGY SAVING TECH DEV CO LTD

Nano-porous aerogel/fiber composite super thermal insulation material and preparation method thereof

The invention discloses a nano-porous aerogel/fiber composite super thermal insulation material and a preparation method thereof. The aerogel/fiber composite super thermal insulation material comprises silicon dioxide aerogel, alumina micro powder, zirconium oxide fibers and opacifying agent of titanium dioxide. The preparation method comprises that organic solvent, cross-linking agents and organic monomers make up pre-mixed solution according to a certain proportion, the silicon dioxide aerogel, the alumina micro powder, the zirconium oxide fibers, pore-forming agents, suspending agents and the titanium dioxide make up slurry through a ball milling process according to a certain proportion, then a certain amount of initiating agents and a certain amount of catalytic agents are dropwise added into the slurry through vacuum bubble removal, composite material in-situ solidification is achieved through a gel injection moulding process, and then demoulding, vacuum drying and degreasing glue discharging are conducted. The nano-porous aerogel/fiber composite super thermal insulation material has a nano-porous/ reinforced fiber composite microstructure, the heat conductivity is 0.040-0.046W*m<-1>*K<-1> (298K), and the flexure strength is as high as 12-14MPa. Preparation processes are simple, industrialized application is easily achieved on a large scale, and the nano-porous aerogel/fiber composite super thermal insulation material is suitable for thermal protection of aerospace, military affairs and severe rugged environments.
Owner:JIANGSU ZHONGLEI ENERGY SAVING TECH DEV CO LTD

Detection method of damage of one-way silicon carbide fiber toughening silicon carbide ceramic matrix composite in oxidation environment

The invention discloses a detection method of damage of one-way silicon carbide fiber toughening silicon carbide ceramic matrix composite in oxidation environment and aims to solve the technical problem that the prior detection method of damage of the one-way silicon carbide (SiC) / SiC composite is bad in accuracy. The technical scheme is that an oxidizing reaction kinetics equation is applied to calculate the thickness of oxidation loss of a carbon interface in the composite material microstructure oxidation process and acquire a geometric model under different oxidation times of the composite microstructure; a finite element model of the composite microstructure after being oxidized is built to conduct finite element calculation of microcosmic stress; and maximum stress strength criterions are adopted to detect damage conditions of materials. The detection method of damage of the one-way silicon carbide fiber toughening silicon carbide ceramic matrix composite in the oxidation environment is simple and high-efficiency from the molding process to the calculation process, overcomes the defects that the prior experimental method is high in cost and long in time consumption, acquires the microcosmic stress in the microstructure of the composite after being oxidized with the help of the strong finite element analysis function of ANSYS; improves accuracy of damage analysis of the one-way SiC / SiC composite and solves the problem that the mesomechanics model is low in accuracy.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Preparation method of graphene coating capable of resisting acid medium corrosion in fuel cell

ActiveCN111446461AQuick Spray OperationEfficient Spray OperationMetallic material coating processesCollectors/separatorsGraphene coatingFuel cells
The invention relates to the technical field of material surface treatment, and in particular relates to a preparation method of a graphene coating capable of resisting acid medium corrosion in a fuelcell. The preparation method comprises the steps of L1 polishing a metal bipolar plate substrate; L2 placing the polished metal bipolar plate substrate into an ultrasonic cleaning pool to be cleaned;L3 placing the metal bipolar plate substrate subjected to ultrasonic cleaning on a substrate rotating stand, and introducing argon to perform glow discharge cleaning on the surface of the metal bipolar plate substrate; L4 gluing the metal bipolar plate substrate subjected to glow discharge cleaning through a polymer conductive adhesive solution pool; L5 evenly adsorbing graphene powder to the surface of the metal bipolar plate substrate through a graphene carbon powder spraying system; and L6 placing the metal bipolar plate substrate with the graphene powder layer in a multi-layer polar plateplacing cabinet. According to the method, a multi-layer composite microstructure and a large number of amorphous structures are formed on the surface of the metal bipolar plate substrate, so that thedensity of the coating is improved, a corrosive medium can be prevented from immersing into the coating, and the corrosion resistance of the coating is greatly improved.
Owner:ZHEJIANG HAROG TECH CO LTD

Preparation method and application of biomedical degradable magnesium alloy surface fine grain composite layer

The invention discloses a preparation method and application of a biomedical degradable magnesium alloy surface fine grain composite layer. The method comprises the steps that a magnesium alloy substrate is subjected to grinding treatment and chemical cleaning; nanometer hydroxyapatite powder is sprayed to the surface of the magnesium alloy substrate in a cold spray mode, and a nanometer hydroxyapatite coating is obtained; and the surface of the magnesium alloy substrate with the nanometer hydroxyapatite coating is subjected to friction stirring machining, and a nanometer hydroxyapatite-fine grain composite structure is formed on the surface of the magnesium alloy. The method is based on a high-efficiency rapid cold spray coating preparation technique and friction stirring machining technique, a nanometer hydroxyapatite-fine grain composite structure layer is prepared on the surface of the magnesium alloy, the method has the advantages of being reasonable in process, low in cost, highin efficiency, environmentally friendly and the like, the corrosion resistance of the biomedical degradable magnesium alloy can be effectively improved, the excellent cellular affinity and osteogenesis function are achieved, the biomedical function of osteoblasts can regulated, the osseointegration capacity is improved, and the method has broad application prospects in the medical fields such as orthopedic implantation.
Owner:CHINA WEAPON SCI ACADEMY NINGBO BRANCH

Composite microstructure current collector for lithium ion battery and preparation method of composite microstructure current collector

The invention discloses a composite microstructure current collector for a lithium ion battery and a preparation method of the composite microstructure current collector for the lithium ion battery. The composite microstructure current collector comprises a smooth bottom surface and a top surface with a composite microstructure; the top surface comprises a micro-convex table and grooves, and the micro-convex table is surrounded by the grooves; concave holes, scaly burrs and a sinking structure are arranged on the micro-convex table. The preparation method comprises the following steps: (1) designing a cutter and carrying out pretreatment on a copper sheet; (2) cutting a processing surface microstructure by a plow. The composite microstructure current collector for the lithium ion battery,disclosed by the invention, can effectively increase the surface area of the current collector to enhance the contact between active materials and the current collector, and improve the utilization ratio of the active materials and the conductivity of an electrode to increase the capacity of the battery, reduce the impedance of the battery, and improve the rate capability of the battery. The composite microstructures such as the grooves, the concave holes, the scaly burrs, the sinking structure and the like can limit acute volume changes of the active materials during the charging-dischargingprocess of the battery to prolong the service life of the battery and improve electrochemical properties of the reversible capacity, the cycling stability, the coulombic efficiency and the like of thebattery.
Owner:SOUTH CHINA UNIV OF TECH

Spray cooling device combining steam cavity and composite microstructure

The invention discloses a spray cooling device combining a steam cavity and a composite microstructure. The device comprises a spray chamber, a spray chamber liquid inlet pipe, a spray chamber liquidoutlet pipe and a steam chamber, wherein the spray chamber and the steam chamber are integrally arranged; the spray chamber comprises a spray orifice plate, array nozzles and a composite microstructure which are positioned in the spray chamber; the spray orifice plate divides the spray chamber into a buffer chamber and a spray chamber; the spray chamber liquid inlet pipe is communicated with the buffer chamber; the spray chamber liquid outlet pipe is communicated with the spray chamber, the composite microstructure is arranged on the wall face, opposite to the array nozzle, in the spray chamber, the composite microstructure comprises a bottom layer liquid absorption core arranged on the wall face opposite to the array nozzle and a plurality of rib-shaped liquid absorption cores arranged onthe bottom layer liquid absorption core, and a phase change working medium is sealed in the steam chamber. The steam chamber expands heat generated by a heat source to the spraying wall face with a large area, the heat exchange performance of the wall face is improved through multi-nozzle array spraying, and the two-phase heat exchange capacity of spraying is improved through combination of the steam chamber and a composite microstructure enhanced heat transfer mode.
Owner:NANJING UNIV OF SCI & TECH

Laser semi-solid processing preparation method of high-strength high-toughness metal material, high-strength high-toughness metal material, and application thereof

The invention belongs to the technical field of metal materials, and particularly relates to a laser semi-solid processing preparation method of a high-strength high-toughness metal material, the high-strength high-toughness metal material, and application thereof. The preparation method comprises the steps of (1) hot-cladding a three-dimensional (3D) forming metal piece layer by layer through a first beam of continuous laser, and acquiring the temperature of a cladding layer in real time; (2) when the temperature of the cladding layer is reduced to be within a semi-solid state area formed bya primary solid phase, carrying out mechanical disturbance on the semi-solid-state cladding layer through a shock wave effect of a second beam of short-pulse laser; and (3) circularly acting on the cladding layer layer by layer, and then cooling naturally until 3D forming a dual-scale/multi-scale composite structure metal component. According to the laser semi-solid processing preparation method of the high-strength high-toughness metal material, the high-strength high-toughness metal material, and the application thereof provided by the invention, the metal material with novel composite microstructures such as dual-scale/multi-scale structures of nano-grain, ultra-fine grain and fine grain and an excellent combination property is obtained, and can be widely applied to the fields such as high speed railway, space flight and aviation, military industry and instruments and apparatus, and the effective control on macroscopical deformation and cracking problems of metal pieces is realized.
Owner:GUANGZHOU INST OF RAILWAY TECH

Binary composite structure type nickel boron alloy coating and preparation method and application thereof

The invention discloses a binary composite structure type nickel boron alloy coating and a preparation method and application thereof. The nickel boron alloy coating is provided with a micron and nanobinary composite microstructure, wherein the first-order structure is a micron-level vortex cell type structure unit; a second-order structure is a nano-level villus type structure unit. The preparation method comprises the steps of chemically coating a surface-cleaned workpiece to be coated in a chemical coating solution to obtain a coated workpiece subjected to chemical coating treatment; and thermally processing the surface of the coated workpiece to obtain the binary composite structure type nickel boron alloy coating. The binary composite structure type nickel boron alloy coating is extremely high in heat dissipating performance, high in corrosion resistance, low in friction coefficient, high in adhesive force, hard to peel off, low in cost, simple in processing processes, and free from pollution, and achieves engineering realization; the service performances of spare parts can be effectively improved; the service life is prolonged; and the binary composite structure type nickelboron alloy coating is applicable to the surface reinforcing processing of a rapid cutting tool or a rapid fire weapon.
Owner:NORTH CHINA UNIVERSITY OF TECHNOLOGY
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