Hollow aluminum oxide ball-based composite abrasive material and preparation method and grinding tool thereof
A technology of hollow alumina and composite abrasives, applied in chemical instruments and methods, abrasives, manufacturing tools, etc., can solve problems such as falling off and not being able to play a good role in grinding
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Embodiment 1
[0039] The preparation method of the hollow alumina ball-based composite abrasive of the present embodiment, the process flow chart is as follows Figure 5 shown, including the following steps:
[0040](1) Gel preparation: Weigh 200g of pseudo-boehmite and add 550ml of deionized water. After ball milling in a ball mill tank for 2 hours, take out the slurry, heat it in a water bath at 75°C, and slowly add 80ml of dilute nitric acid (water , concentrated nitric acid volume ratio=1:7, the concentration of concentrated nitric acid is 65%) after stirring for 20min, add 600 milliliters of magnesium nitrate, lanthanum nitrate, iridium nitrate mixed solution rapidly (wherein the concentration of magnesium nitrate, lanthanum nitrate, iridium nitrate respectively 0.03, 0.01, 0.01mol / L), made into dilute colloid for later use;
[0041] (2) Coating: Weigh 1000g of hollow spherical alumina (particle size 0.5-1.0mm), then weigh 150g of the dilute colloid prepared in step 1), mix the two, a...
Embodiment 2
[0045] The preparation method of the hollow alumina ball-based composite abrasive of this embodiment is basically the same as that of Example 1, the only difference being:
[0046] (1) Gel preparation: After adding dilute nitric acid to form a sol, add 600 milliliters of magnesium nitrate, cerium nitrate, cobalt nitrate mixed solution (wherein the concentrations of magnesium nitrate, cerium nitrate, and cobalt nitrate are 0.03, 0.01, 0.01mol / L respectively ), made dilute colloid for subsequent use;
[0047] (2) Coating: Weigh 1000g of hollow spherical alumina (particle size 0.2-0.5mm), then weigh 100g of the dilute colloid prepared in step 1), mix the two, and wait until the colloid is completely adsorbed on the hollow alumina After the surface of the ball, the whole gluing process ends;
[0048] (4) Furnace firing: Put the dried hollow alumina balls with colloidal particle adhesion layer into the muffle furnace for firing, wherein the temperature of the furnace is raised fro...
Embodiment 3
[0050] The preparation method of the hollow alumina ball-based composite abrasive of this embodiment is basically the same as that of Example 1, the only difference being:
[0051] (1) Gel preparation: After adding dilute nitric acid to form a sol, add 600 milliliters of magnesium nitrate, iridium nitrate, and lanthanum nitrate mixed solution (wherein the concentrations of magnesium nitrate, iridium nitrate, and lanthanum nitrate are respectively 0.03, 0.01, 0.01mol / L ), made dilute colloid for subsequent use;
[0052] (2) Coating: Weigh 1000g of hollow spherical alumina (particle size 1.0-1.5mm), then weigh 180g of the dilute colloid prepared in step 1), mix the two, and wait until the colloid is completely adsorbed on the hollow alumina After the surface of the ball, the whole gluing process ends;
[0053] (4) Furnace firing: put the dried hollow alumina balls with colloidal particle adhesion layer into the muffle furnace for firing, wherein the temperature of the furnace i...
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