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Manufacturing method and application of fly-ash-based aircraft tail flame infrared suppression material

An infrared suppression and fly ash technology, applied in the field of materials, can solve the problems of single evaluation index, slow development, and less research on particle arrangement of granular materials.

Active Publication Date: 2021-09-10
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Traditional fly ash based zeolite / N-TiO 2 The preparation technology of composite materials needs to be loaded on after a series of operation steps after synthesizing zeolite molecular sieve, the cost is high and the operation steps are complicated; the traditional raw materials are usually chemical reagents as the source of silicon and aluminum, which has a certain cost; fly ash The use value in the application field is not high; the infrared radiation suppression method and the materials used for the aircraft plume have little research on the arrangement of particles, and there are few reference materials for structural design optimization. The research and evaluation indicators for particle materials are relatively single. The analysis method is simple, the overall development is relatively slow, and the cost of infrared suppression materials is relatively high

Method used

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  • Manufacturing method and application of fly-ash-based aircraft tail flame infrared suppression material
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  • Manufacturing method and application of fly-ash-based aircraft tail flame infrared suppression material

Examples

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preparation example Construction

[0064] A new material for infrared radiation suppression of aircraft plume—fly ash-based zeolite / N-TiO 2 The preparation method of composite material, comprises the following steps:

[0065] 1) Mix tetrabutyl titanate and absolute ethanol at a volume ratio of 1:1.2~1.5, stir at a rate of 300r / min, stir for 20~50min, record it as solution A, mix 4.5~5.5g of urea with 90 ~120mL of absolute ethanol was mixed to obtain solution B, which was added dropwise into solution A, and decomposed by microwave under 300W for 15~30min to prepare a mixture gel, that is, to obtain a precursor.

[0066] 2) Dry the mixture gel obtained in step 1) at 80-90° C. for 12-15 hours, grind it, and set it aside.

[0067] 3) Calcinate the product obtained in step 2) in a muffle furnace at 400-500°C for 2-3 hours, and obtain N-TiO after cooling 2 composite material.

[0068] 4) Mill the fly ash with a ball mill for 5-10 minutes, and sieve through 300 mesh.

[0069] 5) Prepare an HCl solution with a mass...

Embodiment 1

[0080] Example 1 Coal ash-based zeolite / N-TiO 2 Preparation of composite materials

[0081] 1) Mix tetrabutyl titanate and absolute ethanol at a volume ratio of 1:1.2, stir for 30 minutes, and record it as solution A, mix 5 g of urea with 125 mL of absolute ethanol to obtain solution B, and add solution B dropwise In solution A, the microwave was decomposed under the condition of 300W for 30min to prepare the precursor.

[0082] 2) Dry the precursor obtained in step 1) at 90°C for 12 hours, grind it, and set it aside.

[0083] 3) Calcinate the product obtained in step 2) in a muffle furnace at 450°C for 2.5h, and obtain N-TiO after cooling 2 composite material.

[0084] 4) Fly ash is ball-milled with a ball mill for 5 minutes, and sieved to 300 mesh.

[0085] 5) Prepare an HCl solution with a mass fraction of 20%, mix the fly ash and the HCl solution after sieving 300 meshes in step 4) in a ratio of 1:10 in g:mL, and place on a constant temperature magnetic stirrer with S...

Embodiment 2

[0090] Example 2 Coal ash-based zeolite / N-TiO 2 Application of Composite Materials

[0091] Innovative design of the injection structure of the material on the aircraft, combined with the fly ash-based zeolite / N-TiO prepared in Example 1 2 The characteristics of composite materials are used as anti-red materials, and the structural design of aircraft is as follows: figure 2 As shown, the injection structure is mainly composed of three parts, which are the fuselage 1, the duct 3 and the heat exchange channel 4. The duct 3 is arranged on the fuselage 1 and wraps the tail flame injection channel. Both sides of the duct 3 are provided with a heat exchange channel 4, and the entrance of the heat exchange channel 4 is located behind the entrance of the duct. The duct 3 is ring-shaped, and the middle interior of the duct 3 is the tail flame 6 injection channel, and the middle interior of the duct 3 is set as the air inlet 2, and an air adjustable baffle 9 can be provided at the ai...

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Abstract

The invention relates to a manufacturing method and application of a fly-ash-based aircraft tail flame infrared suppression material. The manufacturing method comprises the steps of S1, manufacturing an N-TiO2 composite material; S2, pretreating fly ash, mixing the pretreated fly ash with an NaOH solid, and then conducting high-temperature calcination to obtain alkali-molten ash; S3, adding deionized water into the N-TiO2 composite material and the alkali-molten ash, mixing the materials, and then conducting aging operation; and S4, crystallizing, filtering, washing and drying the aged materials to obtain the fly-ash-based aircraft tail flame infrared suppression material. The material manufactured according to the manufacturing method realizes the suppression on infrared radiation of a tail flame of an aircraft. A particle spraying pipe is designed to spray particles towards the center of the tail flame, and therefore the zeolite particles and the tail flame gas can be fully mixed, the high-emissivity radiation gas of the tail flame is adsorbed by utilizing the high adsorbability of the particles, the gas radiation characteristic of the tail flame is changed, the purpose that the radiation wave band is located outside the detection range is achieved, and the uncombusted combustible gas is subjected to catalytic oxidation through illumination loaded titanium dioxide to prevent recombustion.

Description

technical field [0001] The invention relates to a preparation method and application of a fly ash-based aircraft tail flame infrared suppression material, belonging to the technical field of materials. Background technique [0002] Fly ash is the pulverized coal of a thermal power plant that is burned in a suspended state to form fine droplets, which are rapidly cooled to form fine particles when passing through the furnace tail, and then collected by a dust collector to obtain fly ash. As a kind of solid waste, fly ash has an annual output of 600-700 million tons, but its comprehensive utilization rate is not high. In order to realize its high-value utilization, fly ash is usually made into zeolite molecular sieves and used in various fields. [0003] TiO 2 As the most commonly used photocatalyst, it has the characteristics of relatively low price and good photocatalytic performance, but on the one hand, TiO 2 Visible light is not very active, so it is usually modified. T...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): F41H3/00
CPCF41H3/00
Inventor 薛海月王连勇刘向宇杨义凡韩建丽何艳
Owner NORTHEASTERN UNIV
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