Method for preparing crystal film through ion beam enhanced corrosion
An ion beam enhancement and crystal technology, applied in phonon exciters, active medium materials, laser parts, etc., can solve the problems of complex process, high cost, and long time for growing crystal thin films.
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Embodiment 1
[0035] A method based on carbon ion beam irradiation enhanced corrosion Yb:YAG crystal film stripping, comprising steps as follows:
[0036] (1) polishing and cleaning the cut Yb:YAG crystal 3;
[0037] (2) The energy emitted by the ion accelerator is 6 Mev, and the dose is 2×10 15 ions / cm2 of carbon ions 1 bombards the polished surface of Yb:YAG crystal, forming a defect layer 2 that is easily corroded below the directly bombarded polished surface;
[0038] (3) the Yb:YAG crystal bombarded by the above ions is cut with a diamond cutter 4, and the bombardment surface is cut to obtain a groove 6 with a depth of 25-50 μm and a width of 100-200 μm; the interval between the two grooves is 20-200 μm, a ridge-shaped protrusion 5 with a width of 20-200 μm is formed between the two grooves, exposing the defect layer;
[0039] (4) 98% concentrated phosphoric acid is mixed with deionized water at a volume ratio of 4:1 to obtain an acid solution 8, which is injected into the quartz ves...
Embodiment 2
[0043] A method based on carbon ion beam irradiation enhanced corrosion Nd:YAG crystal film stripping, comprising steps as follows:
[0044] (1) Polishing and cleaning the cut Nd:YAG crystal 3;
[0045] (2) The energy emitted by the ion accelerator is 6 Mev, and the dose is 2×10 15 ions / cm2 of carbon ions 1 bombard the polished surface of Nd:YAG crystal, forming a defect layer 2 that is easily corroded below the directly bombarded polished surface;
[0046](3) The Nd:YAG crystal bombarded by the above ions is cut with a diamond cutter 4, and the bombardment surface is cut to obtain a groove 6 with a depth of 25-50 μm and a width of 100-200 μm; the interval between the two grooves is 20-200 μm, a ridge-shaped protrusion 5 with a width of 20-200 μm is formed between the two grooves, exposing the surface defect layer;
[0047] (4) 98% concentrated phosphoric acid is mixed with deionized water at a volume ratio of 4:1 to obtain an acid solution 8, and the acid solution 8 is inje...
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