Machine table for depositing high-adhesion film on III-V substrate and a process of machine table

A III-V, high-adhesion technology, applied in metal material coating process, gaseous chemical plating, coating, etc., can solve the problems of reduced adhesion, poor film adhesion, oxygen isolation, etc., to achieve guaranteed Clean, hydrogen-reducing effect

Pending Publication Date: 2021-09-28
JIANGSU LEUVEN INSTR CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] III-V materials, such as InP, GaAs, etc., are very popular in optical communication and 5G, but it is challenging to deposit dielectric films (silicon oxide, silicon nitride) on their substrates. The main problem is the adhesion of films prepared by PECVD. The adhesion is too poor, and finally the blue film process cannot be passed when the device is cut, that is to say, the silicon oxide and silicon nitride adhered to the blue cutting film will be torn off
[0003] At present, PECVD is used to slowly deposit silicon oxide and silicon nitride dielectric films (several A / min) at 200-300°C and <200mTorr cavity pressure, the purpose is to form based on the full reaction of silane, ammonia, laughing gas and other gases Silicon oxide, silicon nitride, reduce the hydrogen content and the number of dangling bonds in the film to make the film dense enough; another reason is that the natural oxide layer formed on the surface of the III-V compound reduces the adhesion; but because the film is deposited at a low speed , Generally, it takes about 20-30 minutes to deposit a film with a thickness of 300-500nm, so it has a great impact on production capacity. Liquid cleaning is done at normal temperature and pressure, which cannot be completely isolated from oxygen, and the sample is easily oxidized again during the drying process

Method used

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  • Machine table for depositing high-adhesion film on III-V substrate and a process of machine table

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] figure 1 As shown, the machine platform for depositing a high-adhesive film on a III-V substrate provided by the present application includes a main chamber 1, a support base 2 is arranged on the top of the main chamber 1, and a lifting device is installed at the bottom of the main chamber 1 4. The lifting device 4 is arranged opposite to the support base 2, and the slide table 3 is installed at the position where the lifting device 4 is opposite to the support base 2; the aforementioned support base 2 is U-shaped, and a catalytic wire is embedded in the U-shaped groove 9. The catalytic wire 9 is a tungsten wire or a graphite wire; one side of the main chamber 1 is respectively provided with a first air inlet 5 and an air inlet 7, wherein the first air inlet 5 is used to feed reaction gas, and the air inlet 7 is connected to the The molecular pump and the dry pump are connected in sequence. Usually, the dry pump and the molecular pump are used as follows. It is the bac...

Embodiment 2

[0050] This application provides a process for depositing a high-adhesion film on a III-V substrate, including a film deposition process and a cleaning process,

[0051] The thin film deposition process includes

[0052] In step 11, the lifting device 4 is started, and the loading table 3 is lowered by the lifting device 4, so that the loading table 3 is far away from the support base 2, and the III-V sample is placed on the loading table 3,

[0053]Step 12, close the main chamber 1, turn on the dry pump and the molecular pump successively, and evacuate the main chamber 1 until the internal pressure of the main chamber 1 is lower than 1mTorr. Oxygen desorption prevents tungsten wire or graphite wire from being oxidized, thus increasing the service life. The temperature of the slide table 3 is kept at 350 °C

[0054] Step 13, feed hydrogen and ammonia into the main chamber 1 through the first air inlet 5, the flow range of the hydrogen feed is 10-200 sccm, and the flow range o...

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PUM

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Abstract

The invention relates to a machine table for depositing a high-adhesion film on an III-V substrate and a process of the machine table. The machine table for depositing the high-adhesion film on the III-V substrate comprises a main chamber, a supporting seat is arranged at the top of the main chamber, a lifting device is installed at the bottom of the main chamber, the lifting device and the supporting seat are oppositely arranged, and a slide holder is installed at the position, opposite to the supporting seat, of the lifting device; the supporting seat is U-shaped, a catalytic wire is embedded in a U-shaped groove of the supporting seat, a first gas inlet and an extraction opening are respectively formed in one side of the main chamber, the first gas inlet is used for introducing reaction gas, and the extraction opening is connected and communicated with a pump body; a second gas inlet is formed in the other side of the main chamber and is communicated with a remote plasma gas generation module; according to the machine table for depositing the high-adhesion film on the III-V substrate and a process of the machine table, process quality can be ensured, and meanwhile, the cleanliness of the chamber is improved.

Description

technical field [0001] The invention relates to a machine platform for depositing a high-adhesive thin film on a III-V substrate and a process thereof, belonging to the field of semiconductor manufacturing. Background technique [0002] III-V materials, such as InP, GaAs, etc., are very popular in optical communication and 5G, but it is challenging to deposit dielectric films (silicon oxide, silicon nitride) on their substrates. The main problem is the adhesion of films prepared by PECVD. The adhesion is too poor, and finally the blue film process cannot be passed when the device is cut, that is to say, the silicon oxide, silicon nitride, etc. adhered to the blue cutting film will be torn off. [0003] At present, PECVD is used to slowly deposit silicon oxide and silicon nitride dielectric films (several A / min) at 200-300°C and <200mTorr cavity pressure, the purpose is to form based on the full reaction of silane, ammonia, laughing gas and other gases Silicon oxide, sili...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C16/50C23C16/458C23C16/46C23C16/455C23C16/54C23C16/40C23C16/34H01L21/67
CPCC23C16/50C23C16/4581C23C16/46C23C16/455C23C16/54C23C16/4408C23C16/4401C23C16/401C23C16/345H01L21/67011
Inventor 邹志文崔虎山范思大任慧群丁光辉吴志浩许开东陈璐
Owner JIANGSU LEUVEN INSTR CO LTD
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