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Method for preparing 2D resin-sodium silicate compositely-enhanced poplar

A composite reinforcement and sodium silicate technology, applied in wood impregnation, wood treatment, impregnated wood, etc., can solve the problems of flammable and perishable application range, poor dimensional stability, low mechanical strength, etc., to ensure organic cross-linking reaction, The effect of low equipment requirements and high reaction efficiency

Active Publication Date: 2021-10-19
CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, poplar wood has defects such as low mechanical strength, poor dimensional stability, and flammability and perishability, which limit its application range. In order to solve various defects in poplar wood properties and increase its added value, many researchers have carried out impregnation modification on it. At present, the method of pressure impregnation is mainly used to press the modifier into the interior of the wood to achieve the purpose of wood reinforcement
However, the existing method has defects such as low impregnation depth and poor uniformity, and when the two impregnating agents react quickly, the molecules have completed polycondensation to form a macromolecular structure, so it is difficult to enter the wood. Therefore, the applicant believes that it can be Development of new impregnation agents to enhance poplar properties

Method used

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  • Method for preparing 2D resin-sodium silicate compositely-enhanced poplar
  • Method for preparing 2D resin-sodium silicate compositely-enhanced poplar

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A 2D resin-sodium silicate composite reinforcing method for poplar wood of the present invention is to first chemically combine the 2D resin with the wood cell wall through the method of negative pressure-positive pressure alternating cycle impregnation, and then impregnate the sodium silicate into the wood. , the sodium silicate reacts and combines with the 2D resin attached to the cell wall to form a physical and chemical joint filling, and the 2D resin-sodium silicate composite reinforced poplar is obtained. The specific test process includes the following steps:

[0028] (1) Pretreatment of poplar wood: The poplar wood is sawed according to specifications: length×width×height is 60mm×60mm×300mm, and the poplar wood is dried to a moisture content of 5%.

[0029] (2) Immerse the 2D resin into poplar wood by dipping: prepare 5000 g of an aqueous solution of 4% 2D resin according to the formula, then put the poplar wood in a closed tank, first vacuum to -0.05MPa and kee...

Embodiment 2

[0033] A method for 2D resin-sodium silicate composite reinforcement of poplar wood is to chemically combine the 2D resin with the wood cell wall through the method of alternating negative pressure-positive pressure impregnation, and then impregnate the sodium silicate into the wood to make the silicon The sodium reacted and combined with the 2D resin attached to the cell wall to form a physicochemical joint filling to obtain a 2D resin-sodium silicate composite reinforced poplar. The specific test process includes the following steps:

[0034] (1) Pretreatment of poplar wood: The poplar wood is sawed according to specifications: length×width×height is 60mm×60mm×300mm, and the poplar wood is dried to a moisture content of 7%.

[0035] (2) Immerse the 2D resin into poplar wood by dipping: according to the formula, prepare 5000g of 2D resin solution with a mass fraction of 6%, then put the poplar wood in a closed tank, first vacuumize to -0.07MPa and keep the pressure for 20min,...

Embodiment 3

[0039] A method for 2D resin-sodium silicate composite reinforcement of poplar wood is to chemically combine the 2D resin with the wood cell wall through the method of alternating negative pressure-positive pressure impregnation, and then impregnate the sodium silicate into the wood to make the silicon The sodium reacted and combined with the 2D resin attached to the cell wall to form a physicochemical joint filling to obtain a 2D resin-sodium silicate composite reinforced poplar. The specific test process includes the following steps:

[0040] (1) Pretreatment of poplar wood: The poplar wood is sawed according to the specifications: length×width×height is 60mm×60mm×300mm, and the poplar wood is dried to a moisture content of 9%.

[0041] (2) Immerse the 2D resin into poplar wood by dipping: according to the formula, prepare 5000g of 2D resin solution with a mass fraction of 8%, then put the poplar wood in a closed tank, first vacuum to -0.09MPa and keep the pressure for 30min...

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Abstract

The invention discloses a method for preparing 2D resin-sodium silicate compositely-enhanced poplar. The method comprises the following steps: firstly, impregnating 2D resin into wood for chemical bonding, and then impregnating sodium silicate into the wood for reacting and bonding with the 2D resin to form physical and chemical combined filling, thereby obtaining the 2D resin-sodium silicate compositely-enhanced poplar. According to the method, the selected 2D resin and sodium silicate are high in reaction efficiency and good in dipping uniformity, and chemical cross-linking reaction is carried out with the poplar wood as a reaction container, so physical and chemical double filling is formed, the loss resistance of the modified poplar wood is enhanced, the defects of high agent loss and low fixation rate after physical filling and not obviously improved mechanical strength of the modified wood after single chemical dipping are overcome, the physical and mechanical properties of the modified poplar are improved, and dimensional stability is greatly enhanced.

Description

technical field [0001] The invention belongs to the technical field of functional improvement of wood, and in particular relates to a method for 2D resin-sodium silicate composite reinforcement of poplar. Background technique [0002] Plantation wood is the main raw material of my country's wood industry. The effective use of plantation wood is of great significance to solve the problems of shortage of wood resources and high import dependence in my country. As one of the four fast-growing forests, poplar is widely distributed, has many species, and has a short rotation period and strong adaptability. It can play a good role in wood processing and utilization and ecological environmental protection in my country. However, poplar has defects such as low mechanical strength, poor dimensional stability, flammability and perishability, which limit its application range. , At present, the method of pressure impregnation is mainly used to press the modifier into the wood to achie...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B27K3/08B27K3/02B27K5/04B27K3/52B27K3/20B27K3/34G01N1/30
CPCB27K3/08B27K3/025B27K5/04B27K3/52B27K3/20B27K3/34B27K3/02G01N1/30
Inventor 左迎峰毕小茜李萍张源吴义强李贤军袁光明
Owner CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY
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