White mustard seed extract as well as preparation method and application thereof
The technology of white mustard seeds and extracts is applied in the field of biomedicine, which can solve the problems of general curative effect and discomfort for long-term use, and achieve the effect of strong inhibitory activity and small side effects.
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[0024] Preparation of white mustard seed extract:
[0025] Sinapis alba: the Sinapis alba L. used in the present invention was purchased from Anqing, Anhui Province, and was identified as the dried mature seeds of Sinapis alba L., a cruciferous plant.
[0026] Extraction and separation of white mustard seed extract: soak and extract white mustard seed with ethanol with a volume fraction of 80%. After leaching for 60 minutes according to the volume ratio of solid to liquid at 1:12, reflux extraction for 120 minutes at an extraction temperature of 70° C. After concentrating and recovering ethanol under reduced pressure, the ethanol extract was obtained, then dissolved in water, extracted three times with ethyl acetate, the extracts were combined, and the solvent was recovered under pressure to obtain the ethyl acetate extract, which is the white mustard extract. Generally speaking, the yield of white mustard seed extraction is generally 1.3-1.7%.
[0027] Preliminary identifica...
Embodiment 1
[0054] Mix white mustard seed extract and starch slurry at a mass ratio of 1:1, pass through a 80-mesh sieve, mix well, add 10% starch slurry, pass through a 14-mesh sieve to granulate, and dry at 52°C until the moisture content is less than 1% , the dry granules are granulated through a 16-mesh sieve. The prepared dry granule is added with 3% magnesium stearate, mixed evenly, compressed into tablets, and the weight of each tablet is controlled to be 0.2g, and the tablets of the white mustard seed extract are obtained.
Embodiment 2
[0056] Vacuum-dry the white mustard extract and make it into powder, mix the white mustard extract and starch in a mass ratio of 2:1, add 0.5% magnesium stearate by total weight, fill it with hard capsules, and control the filling amount At 0.2-0.3g, the capsule of the white mustard seed extract is obtained.
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