Eugenol-sophorolipid nano-emulsion as well as preparation method and application thereof
A nano-emulsion and sophorolipid technology, applied in the field of antibacterial, can solve the problem of no eugenol-sophorolipid nano-emulsion food-borne pathogens, etc., achieve significant antibacterial effect, simple operation method, and broad market prospects
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Embodiment 1
[0037] The preparation of embodiment 1 eugenol-sophorolipid nanoemulsion
[0038] Weigh eugenol and sophorolipid according to the mass ratio of 9:1, dissolve in chloroform, dry the solvent with a nitrogen blower, and dry it in vacuum overnight to completely remove the solvent. 100 μL of distilled water was added drop by drop. After each addition, the mixture was vortexed at 800 rpm for 10 min, and left to balance for 30 min. Control the amount of water added until the proportion of the mixed component of eugenol and sophorolipid is 0.5g / L, the turbidity A600 is 0.2, and the average particle size of the emulsion is 137nm measured by laser nanometer particle size analyzer.
Embodiment 2
[0040] Weigh eugenol and sophorolipid according to the mass ratio of 8:2, dissolve in chloroform, dry the solvent with a nitrogen blower, and dry it in vacuum overnight to completely remove the solvent. 100 μL of distilled water was added drop by drop, and after each addition, the mixture was vortexed at 800 rpm for 10 min, left to balance for 30 min, and set aside. Control the amount of water added until the proportion of the mixed component of eugenol and sophorolipid is 0.5g / L, the turbidity A600 is 0.8, and the average particle size of the emulsion measured by laser nanometer particle size analyzer is 175nm.
Embodiment 3
[0042] Weigh eugenol and sophorolipid according to the mass ratio of 1:9, dissolve in chloroform, dry the solvent with a nitrogen blower, and dry it in vacuum overnight to completely remove the solvent. Add 50 μL of distilled water drop by drop. After each addition, the mixture was vortexed at 800 rpm for 10 min, and left to balance for 30 min. Control the amount of water added until the proportion of the mixed component of eugenol and sophorolipid is 10g / L, the turbidity A600 is 1.0, and the average particle size of the emulsion is 301nm measured by laser nanometer particle size analyzer.
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