A 3D printing diamond/metal matrix composite material and its preparation method and application
A composite material and 3D printing technology, which is applied in the field of composite materials, can solve problems such as the inability to prepare high density, diamond damage, and insufficient performance, and achieve the effects of eliminating structural defects, improving the bonding state, and improving the bonding condition
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Embodiment 1
[0041] Preparation of Core-Shell Structure Doped Diamond
[0042] Using 150μm single crystal diamond particles as the raw material, a polycrystalline diamond transition layer is first deposited on the surface of the diamond particles by chemical deposition. The process is as follows: the mass flow ratio of the incoming atmosphere is CH 4 :H 2 = 2:98, the number of growth is 2 times, and the time of each growth is 20min, and finally a polycrystalline diamond transition layer with a maximum degree of 400nm is obtained.
[0043] Then, a doped diamond outer shell layer is grown on the surface of the polycrystalline diamond transition layer by hot wire chemical vapor deposition to obtain a diamond reinforcement. Deposition process parameters: the distance of the hot wire is 10mm, the thickness of the hot wire is 0.5mm, the growth temperature is 850°C, the deposition pressure is 3KPa, and the thickness of the diamond film is 2μm by controlling the deposition time; during the chemic...
Embodiment 2
[0048] Preparation of Core-Shell Structure Doped Diamond
[0049] Using 150μm single crystal diamond particles as the raw material, a polycrystalline diamond transition layer is first deposited on the surface of the diamond particles by chemical deposition. The process is as follows: the mass flow ratio of the incoming atmosphere is CH 4 :H 2 = 2:98, the number of growth is 2 times, and the time of each growth is 20min, and finally a polycrystalline diamond transition layer with a maximum degree of 400nm is obtained.
[0050] Then, a doped diamond outer shell layer is grown on the surface of the polycrystalline diamond transition layer by hot wire chemical vapor deposition to obtain a diamond reinforcement. Deposition process parameters: the distance of the hot wire is 10mm, the thickness of the hot wire is 0.5mm, the growth temperature is 850°C, the deposition pressure is 3KPa, and the thickness of the diamond film is 3μm by controlling the deposition time; during the chemic...
Embodiment 3
[0056] Preparation of Core-Shell Structure Doped Diamond
[0057] Using 200μm single crystal diamond particles as the raw material, the polycrystalline diamond transition layer is first deposited on the surface of the diamond particles by chemical deposition. The process is: the mass flow ratio of the incoming atmosphere is CH 4 :H 2 = 2:98, the number of growth is 2 times, and the time of each growth is 20min, and finally a polycrystalline diamond transition layer with a maximum degree of 400nm is obtained.
[0058] Then, a doped diamond outer shell layer is grown on the surface of the polycrystalline diamond transition layer by hot wire chemical vapor deposition to obtain a diamond reinforcement. Deposition process parameters: the distance of the hot wire is 10mm, the thickness of the hot wire is 0.5mm, the growth temperature is 850°C, the deposition pressure is 3KPa, and the thickness of the diamond film is 2μm by controlling the deposition time; during the chemical vapor ...
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