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64results about How to "Improve interface binding state" patented technology

A kind of sic-tac coating/matrix synergistically modified c/c composite material and preparation method thereof

The invention discloses a SiC-TaC coating/matrix collaborative modified C/C composite material and its preparation method. The composite material provided by the invention comprises two parts. The portion below the surface of the C/C composite material is the matrix modified portion with the thickness being 0.1-10mm. In addition, carbide in the C/C composite material emerges in gradient distribution. The portion which is deposited on the surface of a carbon material is a coating portion with the thickness being 10-300 microns. The preparation method of the composite material comprises the following steps of: cutting a C/C green body at the density of 0.80g/cm<3>-1.60g/cm<3> into an annular shape or a plate shape, followed by ultrasonic cleaning and drying, placing into a multifunctional CVD furnace, depositing carbide on the surface layer and surface of the C/C green body by controlling deposition parameters, further densifying the green body by the use of pyrolytic carbon so as to obtain the high-density coating/matrix collaborative modified C/C composite material. The main advantages of the invention are as follows: by the penetration of carbide through the surface layer of the C/C composite material, the thermal expansion coefficient of the matrix is raised, the interfacial bonding state is improved, a continuous transition of carbide is formed between the coating and the matrix, and the metallurgical bonding is accomplished between the coating and the matrix.
Owner:CENT SOUTH UNIV

Method for lowering influence on copper interconnection reliability from online WAT testing

The invention provides a method for lowering the influence on the copper interconnection reliability from the online WAT testing. The method comprises the steps that at least one layer of to-be-tested copper interconnection structure comprising a testing component is formed on a semiconductor substrate; a dielectric barrier layer is deposited on the surface of the to-be-tested copper interconnection structure in advance, and a wafer to be tested is obtained; a testing probe penetrates through the dielectric barrier layer and keeps contact with the copper surface of the testing component, and online WAT testing is carried out on the wafer to be tested; surface activation and reduction treatment are carried out on the tested dielectric barrier layer and a small part of copper exposed after making contact with the testing probe through reducing plasma gas; the dielectric barrier layer continues to be deposited to be at the preset thickness. Through the method for combining the pre-deposited dielectric barrier layer serving as an isolation protection layer before the testing with the surface plasma activation and reduction treatment after the testing, defects in copper and dielectric materials are effectively restrained from being generated in the online WAT testing process, and the influence on the copper interconnection reliability from the online WAT testing is lowered significantly.
Owner:SHANGHAI HUALI MICROELECTRONICS CORP

Preparation method and functionalization process for fiber-reinforced hollow nanofiber membrane

The invention discloses a preparation method and functionalization process for a fiber-reinforced hollow nanofiber membrane. The preparation method comprises the following steps: 1) braiding a tubularbraid as a reinforcement by using a two-dimensional braiding technique; and 2) preparing an electrospinning solution, subjecting the prepared electrospinning solution to defoaming, putting the electrospinning solution in an electrospinning device, installing the reinforcement on the receiving unit of the electrospinning device, and carrying out electrospinning under condition of a temperature of15 to 50 DEG C, a relative humidity of 50 to 80%, a positive high voltage of 5 to 35 kV, a negative high voltage of 0 to 10 kV, a solution propulsion speed of 0.2-3 mL / h, a needle inner diameter of 0.16-2.0 mm and a rotating speed of 500-3000 r / min so as to obtain the product with improved mechanical properties. The preparation method is simple in process, low in cost and convenient for industrialimplementation. The functionalization process comprises the following steps: sequentially immersing the fiber-reinforced hollow nanofiber membrane in a modified solution and a metal ion salt solution, and carrying out washing and drying so as to obtain a product having catalytic properties.
Owner:TIANJIN POLYTECHNIC UNIV

Method for preparing high-silicon aluminum alloy by peeling and thermal extruding through rapid-solidified powder metallurgy

The invention relates to a method for preparing high-silicon aluminum alloy by peeling and thermal extruding through rapid-solidified powder metallurgy. The method comprises the following steps: preparing high-silicon aluminum alloy powder through an atomizing powdering method; screening the powder; selecting the high-silicon aluminum alloy powder with average particle being not greater than -150 meshes; transferring into an aluminum covered sleeve; performing air removing and opening sealing; then carrying out peeling and thermal extruding to obtain a high-silicon aluminum alloy bar; machining to remove the aluminum covered sleeve in the periphery of the high-silicon aluminum alloy bar; and performing solid solution treatment and aging treatment to obtain the finished high-silicon aluminum alloy. The high-silicon aluminum alloy material prepared by the method is small and uniform in structure, high in density which can reach 100%, and high in powder deformation, so that the powder interface combination state can be improved; the mechanical property of the alloy can be improved; the strength of the high-silicon aluminum alloy material under room temperature is not less than 450MPa, and the plasticity is not less than 1%.
Owner:GENERAL RESEARCH INSTITUTE FOR NONFERROUS METALS BEIJNG

Preparation process of modified magnesium borate crystal whisker reinforced magnesium-matrix composite material

The invention belongs to the technical field of new materials, in particular to a preparation process for modifying and optimizing magnesium alloy matrix and reinforcing the interphase contact surface and interface aiming at the magnesium borate crystal whisker reinforced magnesium-matrix composite material. The study proves that no obvious interface reaction occurs at the interface of the magnesium borate crystal whisker and the magnesium matrix, and the bonding strength of the interface is not high. By adopting the invention, the interface of the crystal whisker reinforced magnesium-matrix composite material reaches a better bonding state, and the performance of the magnesium borate crystal whisker reinforced magnesium-matrix composite material is improved. The preparation process comprises steps of coating the magnesium borate crystal whisker, preparing the modified magnesium borate crystal whisker prefabricated block, preparing cast composite ingot blank by a vacuum pressure infiltration method; and thermally extruding the ingot blank. The composite material comprises components of aluminium isopropoxide Al(OC3H7)3, distilled water, muriatic acid, magnesium borate crystal whisker, magnesium and the balance of magnesium alloy.
Owner:QINGHAI UNIVERSITY

Preparation method of enhanced chlorinated polyvinyl chloride hollow fiber membrane

InactiveCN106693725AImprove mechanical propertiesSolve the problem of high brittleness and easy wire breakageSemi-permeable membranesPolymer scienceFoaming agent
The invention discloses a preparation method of a chlorinated polyvinyl chloride (CPVC) hollow fiber membrane. The preparation method comprises the following process steps: (1) preparing fibers into a hollow braided tube by adopting a two-dimensional braiding technology, and taking the hollow braided tube as a hollow fiber membrane enhancement body; (2) preparing a CPVC casting solution from the following components in percentage by weight: 15 to 35 percent of CPVC, 5 to 20 percent of pore-foaming agent, 2 to 10 percent of processing aid and 40 to 70 percent of organic solvent, totaling 100 percent; (3) coextruding the hollow braided tube obtained in the step (1) and the CPVC casting solution obtained in the step (2) through an annular spinning nozzle by adopting a co-extrusion compound spinning process, uniformly coating the surface of the hollow braided tube with the casting solution, and fully curing to obtain the enhanced CPVC hollow fiber membrane. The enhanced CPVC hollow fiber membrane prepared by the method has high toughness, is low in production cost, and has a wide practical application prospect; the problem of insufficient mechanical strength of an elemental CPVC hollow fiber membrane can be solved effectively.
Owner:康泽源(天津)科技发展有限公司

Preparation method of enhanced hollow polyvinylidene fluoride fiber membrane

The invention discloses a preparation method of an enhanced hollow polyvinylidene fluoride fiber membrane. The preparation method comprises the following steps: (1) preparation of an enhanceosome: braiding polyacrylonitrile fiber into a hollow braided pipe by adopting a two-dimensional braiding technology; (2) preparation of separation layer casting film liquor: respectively dissolving 5-25wt% polyvinylidene fluoride resin and 5-30wt% of additive into a solvent, stirring and dissolving under the condition of 70-90 DEG C, conducting vacuum defoaming to obtain the separation layer casting film liquor; (3) surface pretreatment of the enhanceosome: cleaning and drying the enhanceosome with a neutral detergent, and then infiltrating the enhanceosome with slight polar organic liquid; and (4) preparation of the enhanced hollow polyvinylidene fluoride fiber membrane: evenly coating the separation layer casting film liquor obtained from the step (2) on the surface of the enhanceosome treated in the step (3), and curing to obtain the enhanced hollow polyvinylidene fluoride fiber membrane. The binding strength of a separation layer on the surface of the enhanced hollow polyvinylidene fluoride fiber membrane prepared by adopting the method and the enhanceosome is high, and the separation layer and the enhanceosome are unlikely to strip, and high-pressure backflushing can be conducted.
Owner:TIANJIN POLYTECHNIC UNIV

CrAlN thermal insulation coating for aluminum alloy piston combustor surface and preparation method thereof

The invention discloses a CrAlN thermal insulation coating for an aluminum alloy piston combustor surface and a preparation method thereof. The CrAlN thermal insulation coating comprises a transitionlayer and a thermal insulation layer from the inside out in order, the transition layer is a CrAl coating, and the thermal insulation layer is a CrAlN coating. The method adopts filtered cathodic vacuum arc technique, takes a CrAl alloy target material (Cr, Al metal target) as the cathode, performs deposition of the CrAl coating on the aluminum alloy surface to form a transition layer, then uses nitrogen as the working gas, and coats the transition layer surface with the CrAlN coating evenly to form the thermal insulation layer. The CrAlN thermal insulation coating provided by the invention not only solves the problem of poor binding force and bearing ability caused by large difference of basic physical properties between the CrAlN coating and the aluminum alloy substrate material, also the coating is uniform and compact, has good film-substrate combination state and hardness up to 40GPa, and shows good high temperature thermal insulation properties and thermal shock resistance in piston thermal load test. The CrAlN thermal insulation coating provided by the invention significantly improves the performance reliability and service life of the aluminum alloy piston, and can meet thehigh power and low emission development requirements of modern engines.
Owner:XIANGTAN UNIV

Titanium carbide-based solid solution metal ceramic and preparation method thereof

The invention discloses titanium carbide-based solid solution metal ceramic and a preparation method thereof. The titanium carbide-based solid solution metal ceramic is composed of a hard phase (Ti, W) C solid solution and an adhesive phase Ni, wherein the composite material powder is prepared by mold pressing forming, degreasing and vacuum sintering; the composite material is synthesized by utilizing Ti powder, W powder, Ni powder and graphite powder as raw materials and performing a high-energy ball milling induced self-propagating reaction under argon protection, and the raw materials comprise the following ingredient by mass percent: 40.60-58.02% of Ti powder, 11.02-29.18% of W powder, 15.00-20.00% of Ni powder and 11.94-15.27% of graphite powder. The preparation of solid solution powder is simple in process, short in cycle, low in energy consumption and easy to control the oxygen content, the hardness of the prepared titanium carbide-based solid solution metal ceramic is 89.0-91.8HRA, the bending strength is not smaller than 1680MPa, and the fracture toughness KIC is not smaller than 12.5MPa.m1 / 2, so that the titanium carbide-based solid solution metal ceramic is suitable for serving as high-speed and high-efficiency cutting tools, hot extrusion molds and heat-resistant, corrosion-resistant and wear-resistant parts and components.
Owner:HUAZHONG UNIV OF SCI & TECH

High-thermal conductivity electronic packaging material and preparation method thereof

The invention belongs to the technical field of electronic packaging materials, and provides a high-thermal conductivity electronic packaging material and a preparation method thereof. The packaging material comprises a reinforcement body comprising diamond grains, pure copper powder and a third component, namely chromium, molybdenum, silicon, titanium or tungsten, wherein the volume percentage of the reinforcement body is 25 to 80 percent and that of the third component is 0.01 to 10 percent. The preparation method comprises the following steps: mixing the reinforcement body, the pure copperpowder and the third component evenly in proportion, and reducing the mixture by hydrogen in a reducing furnace for 1 to 5 hours, at a temperature between 200 and 400 DEG C; feeding the mixed powder in a graphite die and treating the mixed powder by adopting a spark plasma sintering process; vacuumizing the graphite die, heating up the graphite die to between 700 and 1,100 DEG C at a rate of temperature increase of 50 to 200 DEG C / min and pressurizing the graphite die to between 20 and 50MPa; and carrying out heat preservation for 1 to 20 minutes when reaching a sintering temperature and thentaking the packaging material out for demoulding after furnace cooling.
Owner:BEIJING AVIATION MATERIAL INST NO 1 GRP CORP CHINA AVIATION IND
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