The invention relates to the technical field of inorganic non-
metallic materials, discloses a composite
calcium source
calcium zinc phosphate refractory material, a preparation method and application, and aims to solve the technical problems that the reaction is out of control, the water-soluble substance residue is high and the performance is difficult to consider in the preparation of the traditional
calcium zinc phosphate material.
Calcium hydroxide and
calcium carbonate are adopted to form a composite calcium source, and a dynamic time-sharing feeding process is matched and comprises the following steps: firstly, stirring a
phosphoric acid aqueous solution and a
zinc oxide-
calcium hydroxide mixture at 20-35 DEG C for 20-40 minutes to form initial
slurry, then adding
calcium carbonate accounting for 0-30% of the
total calcium mole number at an initial thickening point of the
slurry, continuing to stir for 20-40 minutes, and finally, adding
calcium carbonate accounting for 0-30% of the
total calcium mole number at the initial thickening point of the
slurry; and carrying out suction
filtration, and
drying at 100-110 DEG C for 1.5-2.5 hours to obtain a finished According to the method, the operable time is prolonged by more than 200%, the content of water-soluble substances is reduced by more than 50%, high early strength and structural compactness are both considered, and the method is suitable for the fields of high-end anticorrosive coatings and the like and has remarkable process and performance advantages.