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High-viscosity thermal control material with heat recovery function and preparation method thereof

A heat recovery, high-viscosity technology, applied in heat exchange materials, chemical instruments and methods, etc., can solve the problems of secondary pollutant material utilization rate, thermal performance, poor insulation performance, and inability to discharge air bubbles, and achieve rapid improvement. The effect of heat dissipation capacity, good electrical insulation and fast heat balance

Active Publication Date: 2021-12-24
NO 33 RES INST OF CHINA ELECTRONICS TECHNOOGY GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the high viscosity (viscosity ≥ 3 million cps) of thermal control materials with high thermal conductivity and high pressure resistance, during the preparation process, the material viscosity is high, and the air bubbles cannot be discharged, resulting in poor thermal performance and insulation performance of the product
[0003] Vacuum dispersion technology is usually used in China. This technology uses planetary mixers to control the mixing rate, mixing time, vacuum degree and other process parameters to adjust the degree of product dispersion. This technology is highly mature, but there are many bubbles after mixing and the mixing time is long. , cleaning the stirring paddle will cause secondary pollution to the material, and the material utilization rate is only 90%
[0004] At the same time, the current thermal control materials only have high thermal conductivity and have a single function

Method used

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  • High-viscosity thermal control material with heat recovery function and preparation method thereof
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] The resin is made of silicone gel, the heat recovery agent is acetamide, the heat conduction powder is alumina and boron nitride, the curing agent is low-hydrogen silicone oil, and the catalyst is platinum catalyst. 100 parts by mass of resin, 76 parts by mass of heat recovery agent, 3200 parts by mass of heat-conducting powder, 2 parts by mass of curing agent, and 0.4 parts by mass of catalyst. The preparation process is as follows: the first step is to add resin, heat conduction powder, curing agent, catalyst, and heat recovery agent into the black material barrel in proportion, and the second step is to put the black material barrel into the white barrel with a sponge pad inside; the second step Put the white barrel into the upper and lower platens of the mixing and dispersing equipment in three steps, and adjust the process parameters, pressure 15Mpa, tumbling speed: 130 rpm; rotation speed: 300 rpm; vibration speed: 1300 rpm, time : 18 minutes; the fourth step is t...

Embodiment 2

[0046]The resin adopts silicone resin gel and silicone rubber, the heat recovery agent is myristic acid, the heat conduction powder is boron nitride and graphene, the curing agent is low hydrogen-containing silicone oil, and the catalyst is a platinum catalyst. 100 parts by mass of resin, 70 parts by mass of heat recovery agent, 2800 parts by mass of heat conducting powder, 3 parts by mass of curing agent, and 0.6 parts by mass of catalyst. The preparation process is as follows: the first step is to add resin, heat conduction powder, curing agent, catalyst, and heat recovery agent into the black material barrel in proportion, and the second step is to put the black material barrel into the white barrel with a sponge pad inside; the second step Put the white barrel into the upper and lower platens of the mixing and dispersing equipment in three steps, and adjust the process parameters, pressure 18Mpa, tumbling speed: 140 rpm; rotation speed: 350 rpm; vibration speed: 1500 rpm, t...

Embodiment 3

[0049] The resin uses silicone resin gel, silicone rubber, and silicone oil, the heat recovery agent is acetamide, the heat conduction powder is aluminum oxide, boron nitride, and graphene, the curing agent is low-hydrogen silicone oil, and the catalyst is a platinum catalyst. 100 parts by mass of resin, 60 parts by mass of heat recovery agent, 3000 parts by mass of heat conducting powder, 2.5 parts by mass of curing agent, and 0.5 parts by mass of catalyst. The preparation process is as follows: the first step is to add resin, heat conduction powder, curing agent, catalyst, and heat recovery agent into the black material barrel in proportion, and the second step is to put the black material barrel into the white barrel with a sponge pad inside; the second step Put the white barrel into the upper and lower platens of the mixing and dispersing equipment in three steps, and adjust the process parameters, pressure 18Mpa, tumbling speed: 130 rpm; rotation speed: 330 rpm; vibration ...

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Abstract

The invention belongs to the technical field of thermal control materials, and particularly relates to a high-viscosity thermal control material with a heat recovery function and a preparation method thereof. The high-viscosity thermal control material comprises a resin, a heat recovery agent, heat conduction powder, a curing agent and a catalyst, wherein the mass part ratio of the resin to the heat recovery agent to the heat conduction powder to the curing agent to the catalyst is (8-10): (5-7): (280-320): (0.2-0.4): (0.04-0.08). The high-viscosity thermal control material is fast in thermal balance, high in heat conductivity coefficient, low in thermal resistance, good in electrical insulativity and high in tensile strength, can be attached to the surface of a heating electronic component, has a heat recovery function, and effectively improves the safety and reliability of the electronic component.

Description

technical field [0001] The invention belongs to the technical field of thermal control materials, and in particular relates to a high-viscosity thermal control material with heat recovery function and a preparation method thereof. Background technique [0002] Due to the characteristics of fast thermal balance, high thermal conductivity, low thermal resistance, good electrical insulation, and high tensile strength, thermal control materials have been extensively developed in the thermal control design of electronic components in the fields of aerospace, consumer electronics, and communication equipment. and apply. Since the thermal control material with high thermal conductivity and high pressure resistance has the characteristics of high viscosity (viscosity ≥ 3 million cps), during the preparation process, the viscosity of the material is high, and the air bubbles cannot be discharged, resulting in poor thermal performance and insulation performance of the product. [000...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K5/14C08L83/04C08L83/05C08K5/20C08K3/22C08K3/38C08K5/09C08K3/04
CPCC09K5/14C08L83/04C08K2003/2227C08K2003/385C08L2205/025C08K5/20C08K3/22C08K3/38C08K5/09C08K3/042Y02P70/10
Inventor 王执乾范晋锋白翰林张贵恩王月祥张小刚
Owner NO 33 RES INST OF CHINA ELECTRONICS TECHNOOGY GRP