Antibacterial and antiviral microcapsule as well as preparation method and application thereof
An anti-virus, microcapsule technology, applied in the fields of botanical equipment and methods, applications, fungicides, etc., can solve the problems of time lag, high equipment costs, etc., and achieve cleanliness, wide application range, and good biocompatibility. Effect
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Embodiment 1
[0057] The preparation of embodiment 1 antibacterial and antiviral microcapsules
[0058] This embodiment provides an antibacterial and antiviral microcapsule. The antibacterial and antiviral microcapsules are synthetic resin microcapsules loaded with antibacterial and antiviral active ingredients and modified with functional chemical groups on the surface. Its preparation method is:
[0059] (1) Dissolve 3.80 g of sodium dichloroisocyanurate in 100 mL of ultrapure water at room temperature, filter the resulting liquid, and place it in a cool place away from light for 30 minutes. Add the liquid into 900mL ultrapure water, stir and mix evenly to obtain a sodium dichloroisocyanurate solution with a concentration of 3800ppm;
[0060] (2) Tween 80 with a mass fraction of 2% (the mass fraction of Tween 80 in the system composed of Tween 80 and 500 mL ethyl acetate is 2%) was dissolved in 500 mL ethyl acetate, and then added to (1) The resulting solution was 200 mL and stirred to...
Embodiment 2
[0062] The preparation of embodiment 2 antibacterial and antiviral microcapsules
[0063] This embodiment provides an antibacterial and antiviral microcapsule. The antibacterial and antiviral microcapsules are synthetic resin microcapsules loaded with antibacterial and antiviral active ingredients and modified with functional chemical groups on the surface. Its preparation method is:
[0064] (1) Dissolve 7.45g of sodium hypochlorite in 100mL of ultrapure water at room temperature, filter the resulting liquid, and let it stand in a cool place away from light for 30 minutes. Add this liquid into 900mL ultrapure water, stir and mix evenly to obtain a sodium hypochlorite solution with a concentration of 0.1mol / L;
[0065] (2) Dissolve Span 80 with a mass fraction of 2.5% in 300 mL of dichloromethane, then add 100 mL of the solution obtained in (1) and stir to obtain an emulsified system. Mix melamine and formaldehyde at a ratio of 1:3, heat to 70-80°C, adjust the pH value to 8.1...
Embodiment 3
[0067] The preparation of embodiment 3 antibacterial and antiviral microcapsules
[0068] This embodiment provides an antibacterial and antiviral microcapsule. The antibacterial and antiviral microcapsules are synthetic resin microcapsules loaded with antibacterial and antiviral active ingredients and modified with functional chemical groups on the surface. Its preparation method is:
[0069] (1) Dissolve 0.1 mol of molecular iodine in 100 mL of ethyl acetate at room temperature, filter the resulting liquid with suction, and place it in a cool place away from light for 30 min. Add this liquid into 900mL ethyl acetate, stir and mix evenly to obtain molecular iodine solution;
[0070] (2) the sodium dodecylbenzenesulfonate SDBS that mass fraction is 1.5% is dissolved in 100mL isobutanol, then adds the gained solution in (1) and stirs, in N 2 Reflux and condense under air protection, stir in a 72°C water bath at 1000rpm for 20min to disperse the emulsion evenly, and then sonic...
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